2011Restek Presentation-Overviews
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2011 Restek PRESENTATIONS -OVERVIEW 308p |
2 |
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WHAT’S NEW? GC Columns GC Accessories Sample Preparation Restek 2011 |
4-5 |
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Rxi-624Sil ms (fused silica) |
6-7 |
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Rxi-1HT (fused silica) |
8-9 |
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Rtx-Volatile Amine Column (fused silica) |
10-11 |
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Rtx-DHA Columns (fused silica) |
12-13 |
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Rt-Alumina Bond/CFC Columns(fused silica PLOT) |
14-15 |
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Siltek-stainless steel PLOT Columns |
16-17 |
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Siltek-stainless steel PLOT Columns |
18-19 |
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150 micron ID Columns |
20-21 |
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Rxi-1ms |
22-23 |
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Rtx-200 |
24-25 |
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New SKY Inlet Liners |
26-27 |
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Quechers Extraction Salts |
28-29 |
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Centrifuge 0 foe Quechers |
30-31 |
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Use a small bore capillary |
32-33 |
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Influence of column diameter on separation |
34-35 |
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Influence of diameter on analysis time * |
36-37 |
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Practical Challenges with smaller bore columns.. |
38-39 |
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Scope of implementation of 0.15-0.18 mm ID columns |
42-43 |
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NEW Method vs Old |
44-45 |
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APP - Perfume in 1/2 the time : 100s peaks in 12 minutes |
46-47 |
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2011-Restek-SamplePrep-Overview_1-32.pdf |
48-49 |
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Sample Preparation at 2011 Restek Overview |
48-49 |
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Outline |
50-51 |
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What is Sample Preparation? |
52-53 |
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The Sample Prep Market |
54-55 |
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We want a sample that is: |
56-57 |
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Environmental Market |
58-59 |
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Solid Phase Extraction (SPE) Concepts |
60-61 |
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Why SPE? |
62-63 |
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SPE Tubes |
64-65 |
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SPE Disks |
66-67 |
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More SPE Products |
68-69 |
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Pressurized Fluid Extraction(PFE) |
70-71 |
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ASE®Products |
72-73 |
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Environmental Glassware NEW |
74-75 |
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Environmental Positioning |
76-77 |
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Environmental Developments |
78-79 |
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Food Safety Market |
80-81 |
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Restek’s Total Solution for Food Safety |
82-83 |
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Food Safety Expertise |
84-85 |
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Universal Products |
86-87 |
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Filtration |
88-89 |
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Syringe Filters |
90-91 |
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Thomson Filter Vials |
92-93 |
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Technical Glassware |
94-95 |
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2011-Restek-PharmaProducts-Overview_1-48.pdf |
108-109 |
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Pharmaceutical Restek Chromatography Products 2011 Overview |
108-109 |
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Outline |
110-111 |
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Liquid Chromatography Consumables Market by Geography |
112-113 |
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Liquid Chromatography Consumables Market by Industry |
114-115 |
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Market Assessment - HPLC Demandt |
116-117 |
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Technology Focus - Mass Spectrometry |
118-119 |
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Determining Column Format |
122-123 |
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Restek High Purity LC Columns Lines |
126-127 |
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Restek Column Lines |
128-129 |
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Particle Size to Instrument Fit Chart |
130-131 |
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Capillary Columns Available |
132-133 |
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Restek Reverse Phase Column Listing |
134-135 |
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Multi Modal Analysis of 4-MeImidazoles (4MI or 4-MEI) |
138-139 |
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HILIC Retention |
140-141 |
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Reverse Normal Phase / HILIC Column Listing |
142-143 |
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Restek UHPLC |
144-145 |
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Pinnacle DB UHPLC Columns |
146-147 |
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Proper Filtration for uHPLC |
148-149 |
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Product Focus |
150-151 |
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Restek Product Positioning |
152-153 |
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Competitive Column Offerings |
154-155 |
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Selectivity on any Insteument Format |
156-157 |
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The Value of Selectivity |
158-159 |
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USLC Phases have the highest range of selectivity for RPC |
160-161 |
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Great for Column Switching |
162-163 |
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Biphenyl Advantage |
164-165 |
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Viva -Wide-Pore Silica for Bio Pharma |
166-167 |
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BJH Desorption dV/dDPore Volume |
168-169 |
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Viva Competitive Comparison |
170-171 |
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Guard Columns - a necessity |
176-177 |
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Guard Column Options |
178-179 |
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Other LC interesting products |
180-181 |
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GC in Pharmaceutical Market |
182-183 |
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Rxi-3-in-1 Technology |
184-185 |
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Balanced Inertness |
186-187 |
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Highest Thermal Stability of its Class |
190-191 |
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Rxi Essentials for Pharma Use |
192-193 |
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Rxi Updated Brochure |
194-195 |
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USP<467> Standards |
196-197 |
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GC Column Mix for Pharma Method Development |
200-201 |
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Summary |
202-203 |
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2011-RestekPetro-Applications-Overview_1-37.pdf |
204 |
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2011 Restek Petrochemical APPLICATIONS - Overview |
204 |
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Petrochemical |
204 |
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Who are the End-users |
204 |
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Products analyzed in Segment |
204 |
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Outline |
205 |
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Refinery Process Map |
205 |
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What does every refinery do? |
205 |
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Simulated Distillation |
206 |
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Challenges |
206 |
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Needs for Accurate Simulated Distillation Analysis |
206 |
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Sim Dist with fused silica: Big Problem area.. |
207 |
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Optimize strength/robustness of capillaryApplication of MXT Metal capillary tubing |
207 |
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MXT Tubing is Extremely Strong |
207 |
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New, easy accessible column cage |
208 |
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Simulated Distillation of Crude oil |
208 |
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ASTM Spec for High Temperature Sim Dist |
208 |
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Resolution new MXT-1HT Sim Dist |
209 |
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Comparison of Resolution values |
209 |
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Resolution values |
209 |
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Column Stability / Lifetime |
210 |
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Comparison of Bleed values |
210 |
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Performance-ASTM D7169 |
210 |
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C10-C100 calibration standard |
211 |
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Calibration curve C10-C100 |
211 |
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Column Cutting |
211 |
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MXT Column Cutting |
212 |
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Carrier gas considerations : Avoid introduction of oxidizers |
212 |
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Impact of Oxygen/ Moisture |
212 |
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Carrier Gas purification |
213 |
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Simulated Distillation of Gasoline Range Hydrocarbons |
213 |
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D2887 Used for: |
213 |
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Gasoline Range Sim Dist |
214 |
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D-2887 Sim Dist |
214 |
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Restek New Generation MXT Sim Dist Columns |
214 |
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Product information for MXT Sim Dist |
215 |
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Analysis: Gasoline Detailed Hydrocarbon Analysis (DHA) D6730 |
216 |
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Biggest Challenges for Customers Running ASTM D6730 |
216 |
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Why do the Refiners Run DHA Analysis? |
216 |
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Important Quality Parameter for DHA Analysis |
217 |
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Elution of Alcohols on the DHA-type Columns ASTM Method D6730 |
217 |
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Impact of a Tailing Alcohol Peak |
217 |
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ASTM D 6730 Specifications |
218 |
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Standard ASTM-Specs Test for all Restek Rtx-DHA 100 Columns |
218 |
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Specs Data is Listed on each Rtx-DHA-100 Test Report |
218 |
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Reproducibility of Rtx-DHA-100 Columns |
219 |
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ASTM D 6730 Requires a “tuned”Column… |
219 |
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ASTM 6730 DHA Evaluation Mix |
220 |
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Focusing on Critical Areas of Resolution |
220 |
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Gasoline Analysis Following ASTM D6730, Helium as carrier gas |
220 |
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There will be always a wish from customers to SPEED UP the analysis |
221 |
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Using Helium and a different program |
221 |
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Speeding up the Application using HYDROGEN Carrier Gas |
222 |
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Fast DHA Analysis using Hydrogen… |
222 |
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Fast DHA using Hydrogen |
222 |
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Hydrogen : Safety Issues |
223 |
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Rtx-DHA Columns for Other ASTM Methods |
223 |
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Biggest Challenges for customers running ASTM D6730 |
223 |
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Customer referral |
224 |
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Product information Rtx DHA columns |
224 |
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What does every refinery do? : Benzene / Toluene/ ethanol in gasoline |
224 |
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Benzene / Toluene/ ethanol in gasoline |
225 |
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Modified ASTM D3606 Method using the D3606 Column Set |
225 |
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New D3606 Method |
225 |
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Repeatability of 4 Injections of Wallmart Gasoline |
226 |
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Product Information for D3606 |
226 |
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What does every refinery do? : Refinery gases |
226 |
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Refinery Gases |
227 |
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Restek PLOT Columns Versus Competitor Columns |
227 |
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PLOT Layer is often deposited as non homogeneous film |
228 |
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This was one of the reasons why we could replace Varian and Agilent PLOT columns for: |
228 |
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Transportation |
228 |
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Refinery Gas Analysis : AluminaBOND |
229 |
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Difference Between Na2SO4and KCl |
230 |
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C1-C5 Hydrocarbons Rt-Alumina BOND |
229 |
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Difference Between Na2SO4 and KCl |
230 |
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ASTM D2163 C1-C5 Hydrocarbons |
230 |
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Permanent Gases on Rt-MSieve 5A |
230 |
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Rt-Q-BOND Peak Shape for CO2 and C2 Isomers |
231 |
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Permanent Gases, CO and CO2 on ShinCarbon Micropacked Column.. |
231 |
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Product Information for PLOT |
232 |
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Additional UNIQUE Restek Development |
232 |
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MXT-MSieve 5A |
232 |
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Molecular Sieve 5A in MXT |
233 |
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Zooming into some details |
233 |
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MXT-Alumina BOND(Na2SO4 deactivation) |
233 |
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Refinery gas sample |
234 |
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Acetylene and Propadiene |
234 |
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MXT Q-BOND |
235 |
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Solvent Test on MXT-Q-BOND |
235 |
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Peak Shape of Alcohols |
234 |
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Peak Shape for CO2and C2Isomers |
235 |
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Product information MXT PLOT |
236 |
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What does every refinery do? : Sulfur analysis |
236 |
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Reference |
236 |
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All parts in the GC system that come in contact with sulfur compounds can be deactivated by the Siltek technology... |
237 |
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Sulfur Gases at 19 ppb |
237 |
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Most Important Issue for Trace Sulfur Analysis : System Inertness |
237 |
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Rt-XL Sulfur : Sulfurs and Hydrocarbon Analysis of Natural Gas / Refinery Gas at 50 ppb level |
238 |
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Untitled |
239 |
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Trace H2S and COS in Ethylene/Propylene using Selective Detection |
238 |
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Product information Sulfur |
239 |
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What does every refinery do? Oxygenates |
239 |
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Oxygenates in Gasoline Analyses: ASTM D4815 |
239 |
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Product Information for Oxygenates |
240 |
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Food Safety |
242-243 |
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Consumer Pressure - melamine, bisphenol A, mycotoxins, vet drugs, acrylamide, pesticides, PAHs, Dioxins, 4MEI |
246-247 |
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Global Economy |
256-257 |
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Some statistics |
258-259 |
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What challenges arise for the chemist > Trace analysis |
260-261 |
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Function or Chemical Class |
262-263 |
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Pesticide Residues in Foods |
266-267 |
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Veterinary Drugs |
286-287 |
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QuECh-ingf or Beginners |
298-299 |
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What is QuEChERS? |
300-301 |
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Complete Line of QuEChERS Products |
320-321 |
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Other Applications for QuEChERS |
330-331 |
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QuEChERS and Cartridge SPE Cleanup for Pesticides in Dietary Cleanup for Pesticides in Dietary Supplements |
340-341 |
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Sample Preparation of Cannabinoids in Urine Using the QuEChERS Method |
342-343 |
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Restek Technical Information Available at restek.comFood, Flavors, and Fragrances |
348-349 |
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Chlorinated Dioxins and Furans in FoodRestek GC Selectivity Solutions |
350-351 |
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Dioxin contamination scandal hits Belgium |
362-363 |
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Polychlorinated Biphenyls in Food |
364-365 |
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GC Selectivity QuestionsPolycyclic Aromatic Hydrocarbons |
372-373 |
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HPLC of PAHs |
386-387 |
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Restek UHPLC of PAHs –Very Fast Run |
390-391 |
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Summary of Food Safety |
392-393 |
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Other Topics for Food Safety |
396-397 |
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Environmental Program |
404-405 |
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Outline•Semivolatile organic compounds•Volatile organic compounds•Pesticide •Air sampling |
406-407 |
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Semivolatile Overview |
408-409 |
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SemivolatileAnalysisRxi-5Sil MS |
432-433 |
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Rxi-5ms and Rxi-5Sil MS columns are not the same |
436-437 |
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RXi - Value to Customer |
438-439 |
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SemivolatileStandards |
440-441 |
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Injection Ports |
442-443 |
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Sample Extraction for Semi-Volatiles |
450-451 |
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Polycyclic Aromatic Hydrocarbons (PAHs) |
452-453 |
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General Chromatography Supplies |
458-459 |
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Volatile Analysis•How laboratory is set-up•Analysis of volatile compounds–Rtx-VMS–Rxi-624Sil MS•Instrument maintenance |
460-461 |
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Volatiles Overview |
462-463 |
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Analysis for Volatiles GC Columns |
468-469 |
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Rtx-VMS advantages over other phases |
478-479 |
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624 Phase Disadvantage |
480-481 |
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Standards for Volatiles |
494-495 |
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Sample Preparation for Volatiles |
496-497 |
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General Chromatography Supplies |
500-501 |
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Pesticide Analysis |
506-507 |
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Chlorinated Pesticide Overview |
506-507 |
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PesticideAnalysis |
504-505 |
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Rxi-5Sil MS GC Column Technology |
512-513 |
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Injection Ports |
520-521 |
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Variation of Inlet Liners |
524-525 |
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For Most Inert Inlet System |
530-531 |
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Consumable Products for Pesticides |
532-533 |
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Sample Extraction for Pesticides |
534-535 |
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SPE Products for Specific Compounds |
536-537 |
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Extract Clean-up for Pesticides |
538-539 |
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Reference Materials for Pesticides |
540-541 |
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General Chromatography Supplies |
544-545 |
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AIR SAMPLING |
548-549 |
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Air Monitoring Overview |
548-549 |
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Sample Collection Preparation(Canisters) |
554-555 |
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Passive Sampling w/Canisters |
556-557 |
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Sample Collection -Canisters |
558-559 |
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Sample Collection –CanistersTimer |
560-561 |
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Sample Preparation -Canisters |
562-563 |
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Analysis |
564-565 |
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Sample Collection –Mini Canisters |
566-567 |
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Sample Collection Preparation(Thermal Desorption Tubes) |
568-569 |
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Sample Collection –TDU Tubes |
570-571 |
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Sample Collection Preparation(Gas Sampling Bags) |
572-573 |
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SemivolatileAir Sampling(XAD2 & PUFs) |
574-575 |
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Other Air Sampling Products |
576-577 |
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Marketing Literature |
578-579 |
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Sample Process for Air Analysis |
550-551 |
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AIR SAMPLING |
546-547 |