140-141 / 582
Ultra Silica
2.1 x 100mm, 3µm
0.4mL/min
80% MeOH
20% 10mM ammonium formate in water
30ºC
1µL injection
10µg/mL in 0.1% formic acid in water
SIM m/z=83
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
0.00
0.25
0.50
0.75
1.00
1.25
(x1,000,000)
83.00 (1.00)
TIC
k ~ 0.5
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
8.0
9.0
10.0
11.0
12.0
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
8.0
9.0
(x100,000)
83.00 (1.00)
TIC
Ultra PFPP
2.1 x 100mm, 3µm
0.4mL/min
30% Water w/
0.02
% formic acid
70% MeOH
w/
0.02
% formic acid
30ºC
1µL injection
10µg/mL in 0.1% formic acid in water
SIM m/z=83
k ~ 13
HILIC Retention
17