restekapp07 - page 242

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Description
codeine
hydrocodone
hydromorphone
levorphanol
meperidine
methadone
morphine
oxycodone
oxymorphone
Concentration
1000µg/ml
1000µg/ml
1000µg/ml
1000µg/ml
1000µg/ml
1000µg/ml
1000µg/ml
1000µg/ml
1000µg/ml
cat.#
34000
34002
34063
34003
34004
34005
34006
34007
34065
Product Listing:
Rtx
®
-5
30m, 0.25mm ID, 0.25µm (cat.#10223)
Pharmaceutical
standards
All standards are
diluted inmethanol.
Packaged 1ml
per ampul.
For a complete list ofRestek’sQuantitativeDrugStandards,
please request a copy of ourGeneral Catalog.
opiates chromatographwell on a low
polarity (Rtx
®
-5) columnwithgood
resolution andpeak shape.
Sensitivity and specificity in confirming
thepresenceof opiates indifferent
samples canbe enhancedby selectively
choosing certain ions tomonitor.
Identificationbasedupon thepresence
of distinctive, highmass ions is
preferred, especiallywhen analyzing
derivatizedcompounds.Trimethylsilyl
derivativeswill add72 amu for every
hydroxyl groupderivatized.
Effectiveprotocols for opiate analysis
include extensive samplepreparation
andoptimized instrument parameters.
Derivative formation and theuseof
deactivatedglassware, samplevials, and
inlet linerswill ensuremaximum
recoveries and response.Optimized
detector parameters using selected ions
for detectionwill aid in the identifica-
tionof different compounds.
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