678
GC CHROMATOGRAMS |
FORENSIC/PHARMACEUTICAL
Barbi turates
6 7 5
Column:
Rtx
®
-35, 30m, 0.53mm ID, 1.0µm (cat.# 10455)
Sample:
1.0µL splitless injection of acidic/neutral drugs
Conc.:
50µg/mL
Oven temp.:
100°C to 280°C @ 10°C/min. (hold 5 min.)
Inj./det. temp.:
250°C
Carrier gas:
helium
Linear velocity:
40cm/sec. set @ 100°C
FID sensitivity:
5.12 x 10
-10
AFS
Splitless hold time: 0.5 min.
Barbiturates (Acidic/Neutral Drugs) (Underivatized)
Rtx®-35
1
2
3
4
8
9
11
10
12
13
16
15
14
min.
0
5
10
15
20
GC_PH00262
1. ethosuximide
2. barbital
3. methyprylon
4. aprobarbital
5. butalbital
6. amobarbital
7. pentobarbital
8. secobarbital
9. meprobamate
10. carisoprodal
11. glutethimide
12. phenobarbital
13. methaqualone
14. primidone
15. carbamazepine
16. diphenylhydantoin
Column:
Rtx
®
-1701, 15m, 0.53mm ID, 0.50µm (cat.# 12037)
Sample:
1.0µL splitless injection of acidic/neutral drugs
Conc.:
50µg/mL concentration
Oven temp.:
100°C to 280°C @ 7°C/min.
Inj./det. temp.:
250°C/275°C
Carrier gas:
helium
Linear velocity:
40cm/sec. set @ 100°C
FID sensitivity:
5.12 x 10
-10
AFS
Splitless hold time: 0.5 min.
6 7
Barbiturates (Acidic/Neutral Drugs) (Underivatized)
Rtx®-1701
1
3
2
4
5
8
11
9
15
10
12
13
14
16
min.
0
5
10
15
20
GC_PH00263
Website :
E-mail :
TelNo : 03 9762 2034 . . . in AUSTRALIA
Mar 2011
