Chromatography Columns 2013+ - page 115

58
GCCOLUMNS |
GENERALPURPOSECOLUMNS
Rtx®-Wax
similar
phases
DB-WAX, HP-Wax
free
literature
SelectionGuide for
PolarWaxGC
ColumnPhases
Downloadyour free
copy from
lit. cat.#59890
*Maximum temperatures listed are for 15- and 30-meter lengths. Longer lengthsmay have a slightly reduced
maximum temperature.
Rtx®-WaxColumns
(fusedsilica)
(polar phase; Crossbond®Carbowax®polyethyleneglycol)
• Best polyethylene glycol (PEG) phase for alkenols, glycols, and aldehydes.
• Temperature range: 20 °C to250 °C.
• Equivalent toUSPG14,G15,G16,G20,G39phases.
Rtx®-Wax columns are themost inert and efficient PEG columns currently available.
Theextendedoperating temperature rangeallowsanalysisof compoundshavingawide
volatility range, and ensures low bleed at temperatures as high as 250 °C. Selectivity is
comparable to other Carbowax® columns, for compounds of intermediate to high
polarity. Selectivitydata available on request.
CleaningsolventsonanRtx®-Waxcolumn.
Column:
Rtx
®
-Wax, 30m, 0.32mm ID, 0.25µm (cat.# 12424)
Sample:
1% each solvent inmethanol
Inj.:
1.0µL split (split ratio 100:1), 4mm inlet liner (cat.# 20814)
Inj. temp.:
250°C
Carrier gas:
hydrogen, constant flow
Flow rate:
3.0mL/min.
Oven temp.:
35°C (4min. hold) to 85°C@ 3°C/min., to 200°C@ 15°C/min. (2min. hold)
Det.:
FID@ 250°C
1. methanol
2.
iso
-propanol
3. ethanol
4.
n
-propanol
5.
iso
-butanol
6.
n
-butanol
7. methyl Cellosolve
®
8. limonene
9. Cellosolve
®
10. butyl Cellosolve
®
11. dipropylene glycol monomethyl ether (DPGMME)
12. diethylene glycol ethyl ether (DEGEE)
13. ethylene glycol
14. tripropylene glycol monomethyl ether (TPGMME)
15. phenyl Cellosolve
®
GC_FF00644
ID
df
temp. limits*
15-Meter
30-Meter
60-Meter
0.25mm 0.25µm 20 to 250°C 12420
12423
12426
0.50µm 20 to 250°C 12435
12438
12441
0.32mm 0.25µm 20 to 250°C 12421
12424
12427
0.50µm 20 to 250°C 12436
12439
12442
1.00µm 20 to 240/250°C 12451
12454
12457
0.53mm 0.25µm 20 to 250°C 12422
12425
0.50µm 20 to 250°C 12437
12440
12443
1.00µm 20 to 240/250°C 12452
12455
12458
ID
df
temp. limits
10-Meter
20-Meter
0.10mm 0.10µm 20 to 250°C 41601
41602
0.20µm 20 to 240/250°C 41603
41604
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Mar 2011
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