Chromatography Columns 2013+ - page 110

53
GCCOLUMNS |
GENERALPURPOSECOLUMNS
Rtx®-440
OrganochlorinePesticides (USEPAMethod8081A)onanRtx®-440column.
restek
innovation
!
1. hexachlorocyclopentadiene
2. 2,4,5,6-tetrachloro-m-xylene (SS)
3.
cis
-diallate
4.
trans
-diallate
5.
α
-BHC
6. hexachlorobenzene
7.
γ
-BHC
8.
β
-BHC
9.
δ
-BHC
10. heptachlor
11. aldrin
12. isodrin
13. heptachlor epoxide
14. 2,4'-DDE
15.
γ
-chlordane
16.
α
-chlordane
17. endosulfan I
18. 4,4'-DDE
19. 2,4'-DDD
20. dieldrin
21. chlorobenzilate
22. endrin
23. 2,4'-DDT
24. 4,4'-DDD
25. endosulfan II
26. kepone
27. endrin aldehyde
28. 4,4'-DDT
29. endosulfan sulfate
30. methoxychlor
31. endrin ketone
32. mirex
33. decachlorobiphenyl (SS)
Column:
Rtx
®
-440 30m, 0.32mm ID, 0.50µm (cat.# 12939)
Sample:
Organochlorine PesticidesMix AB#2 (cat.# 32292),
8-80µg/mL each component in ethyl acetate
Chlorobenzilate (cat.# 32211) 1,000µg/mL inmethanol
Diallate (cis & trans) (custom) 1,000µg/mL in hexane
Hexachlorobenzene (cat.# 32231) 1,000µg/mL in acetone
Hexachlorocyclopentadiene (cat.# 32232) 1,000µg/mL inmethanol
Isodrin (custom) 1,000µg/mL in hexane
Kepone (custom) 1,000µg/mL in hexane
Mirex (custom) 1,000µg/mL in hexane
2,4'-DDD (cat.# 32098) 1,000µg/mL inmethanol
2,4'-DDE (cat.# 32099) 1,000µg/mL inmethanol
2,4'-DDT (cat.#32200) 1,000µg/mL inmethanol
TCMX (cat.# 32027) 200µg/mL in acetone
DCB (cat.# 32029) 200µg/mL in acetone
Inj.:
1.0µL splitless (hold 0.75min.), 2mm Siltek
®
treated single gooseneck inlet liner (cat.# 20961-214.1)
Inj. temp.:
275°C
Carrier gas:
hydrogen, constant pressure
Linear velocity: 51 cm/sec.@ 140°C
Oven temp.:
140°C (hold 1min.) to 240°C@ 30°C/min.
(hold 2min.) to 330°C@ 30°C/min.
(hold 4min.)
Det.:
ECD@ 330°C
Instrument:
ShimadzuGC-2010with ECD
GC_EV00796
Rtx®-440Columns
(fusedsilica)
(midpolarityproprietaryCrossbond®phase)
• General purpose columnswithunique selectivity for pesticides, PAHs, or other
semivolatiles. Ideal for low/trace level analyses.
• Lowbleed, high-resolution columnswithunique selectivity.
• Wide temperature range: 20 °C to340 °C.
ID
df
temp. limits
30-Meter
0.25mm 0.25µm 20°C to 320/340°C 12923
0.50µm 20°C to 320/340°C 12938
0.32mm 0.25µm 20°C to 320/340°C 12924
0.50µm 20°C to 320/340°C 12939
0.53mm 0.50µm 20°C to 320/340°C 12940
1.00µm 20°C to 320/340°C 12955
ID
df
temp. limits
20-Meter
40-Meter
0.18mm 0.18µm 20°C to 320/340°C 42902
42903
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Mar 2011
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