CLINICAL/FORENSICS
16
Sympathomimetic Amines
GC
free
literature
HighPerformance Silica
Products
lit. cat.# 59901
OperatingHints for Using
Split/Splitless Injectors
lit. cat.# 59880A
ImprovedGCAnalysis of Basic
Organic CompoundsUsing
BaseDeactivatedColumns&
Liners.
lit. cat.# 59108
GenuineRestek Replacement
Parts for Agilent GCs
lit. cat.# 59627E
Call Restek at 800-356-1688 or
814-353-1300, ext. 5, or con-
tact your Restek representa-
tive, to request your free copy!
Rtx
®
-35 Amine 30m, 0.25mm ID, 0.50µm (cat.# 11338)
1.0µL split injection of underivatized sympathomimetic amines
Conc.
1000ng/µL
Inj. temp:
250°C
Carrier gas:
helium
Linear velocity:
30cm/sec.
Oven temp.:
150°C to 240°C@ 7°C/min.
Det.:
MSD
Scan range:
40–450amu
Ionization:
EI
Mode:
scan
SympathomimeticAmines (Underivatized)
Rtx®-35Amine
GC_PH00574
1. amphetamine
2. methamphetamine
3. N-ethylamphetamine
4.
p
-methoxyamphetamine (PMA)
5.
p
-methoxymethamphetamine (PMMA)
6. methylenedioxyamphetamine (MDA)
7. methylenedioxymethamphetamine (MDMA)
8. methylenedioxyethylamphetamine (MDEA)
9. HMMA
10. MBDB
SympathomimeticAmines (Derivatized)
Rtx®-200
1. phenylethylamine
2. amphetamine
3. phentermine
4. methamphetamine
5. fenfluramine
6. mephentermine
7. cathinone
8. phenylpropanolamine
9. methcathinone
10. nicotine
11. ephedrine
12. pseudoephedrine
13. phenmetrazine
14. phendimetrazine
15. methylenedioxyamphetamine
16. diethylpropion
17. methylenedioxymethamphetamine
18. methylenedioxyethylamphetamine
19. 4-methyl-2,5-dimethoxyamphetamine
20. phenylephrine
21. caffeine
22. benzphetamine
min.
5
7.5
10
12.5
15
17.5
10
14
3
1,2
16
4
8
11
9
7
5
12
13
22
15,20
19 17
18
21
30m, 0.25mm ID, 0.50µmRtx
®
-200 (cat.# 15038)
split mode, split vent flow rate 45mL/min.
Oven temp.:
100°C to 310°C@ 10°C/min.
Varian 3400GC coupledwith Varian Saturn 2000MS detector
Mass spectroscopy data collected using a scan range of 40 amu through 600 amu.
Ionization performed in the EI Automode.
GC_PH00439
