CLINICAL/FORENSICS
9
Basic Drugs (Mixed)
GC
7
30m, 0.25mm ID, 0.25µmRtx
®
-200 (cat.# 15023)
1.0µL split injection of a basic drugmix (1mg/mL)
Conc.:
1000ng/µL
Oven temp.:
100°C to 325°C@ 4°C/min. (hold 10min.)
Inj. / det. temp.:
250°C / 320°C
Carrier gas:
helium
Linear velocity:
30cm/sec. set@ 100°C
FID sensitivity:
1.28 x 10
-10
AFS
Split ratio:
50:1
1
2
4
6
8
10
11
3,5
14
19
17
18
22
23
21
20,25
24
30
28,29
27
37
34
33 36 38
35
31,32
26
16
15
13
12
9
min. 10
20
30
40
50
60
GC_PH00237
MixedBasicDrugs (Underivatized)
Rtx
®
-200
1. nicotine
2. benzocaine
3. cotinine
4. meperidine
5. caffeine
6. benzphetamine
7. ketamine
8. diphenhydramine
9. lidocaine
10. phenyltoloxamine
11. tripelennamine
12. phenothiazine
13. dextromethorphan
14. methadone
15. amitriptyline
16. trimipramine
17. tetracaine
18. pyrilamine
19. medazepam
20. bupivacaine
21. scopolamine
22. codeine
23. morphine
24. diazepam
25. chlorpromazine
26. temazepam
27. flunitrazepam
28. bromazepam
29. prazepam
30. acetopromazine
31. flurazepam
32. papaverine
33. clonazepam
34. haloperidol
35. alprazolam
36. triazolam
37. thioridazine
38. trazodone
MixedBasicDrugs (Underivatized)
Rtx
®
-35
min.
10
20
30
40
50
60
1
2
3
4
6
8
9
10
7
5
11
38
36
37
35
33
34 32
30
27
29
23
26
24
25
22
21
19
18,20
15 14
12 17
16
13
GC_PH00236
30m, 0.25mm ID, 0.25µmRtx
®
-35 (cat.# 10423)
1.0µL split injection of a basic drugmix (1mg/mL)
Conc.:
1000ng/µL
Oven temp.:
100°C to 325°C@ 4°C/min. (hold 10min.)
Inj. / det. temp.:
250°C / 320°C
Carrier gas:
helium
Linear velocity:
30cm/sec. set@ 100°C
FID sensitivity:
1.28 x 10
-10
AFS
Split ratio:
50:1
31
28
