RtxPresentations07 - page 334-335

Analytical ReferenceMaterials
Obtainingpure, neat compounds for the preparation of calibration standards
can be verydifficult. Some of these compounds are not available
commercially at a high enoughpurity for accurate analytical results. These
materials can contain desensitizing agents, such as beeswax, water,
plasticizers, or othermanufacturingby-products.
Manycommerciallyavailable
explosives are shippedwet andmust bedried carefullybefore solution
preparation.
To ensure the highest qualityexplosive standards, Restek chemists carefully
purified or synthesized all of the compounds listed inMethod 8095. All
compounds used toprepare these standards have 98%purityor higher.
Multiple analytical techniques, includingGC, HPLC, GC/MS, FTIR, and
DSC, are used to verify rawmaterial purity.
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