6mx 0.53mmRestekRtx-TNTColumns
1 Nitrobenzene
2 2-Nitrotoluene
3 3-Nitrotoluene
4 4-Nitrotoluene
5 Nitroglycerin
6 1,3-Dinitrobenzene
7 2,6-Dinitrotoluene
8 2,4-Dinitrotoluene
9 3,4-Dinitrotoluene
10 1,3,5-Trinitrobenzene
11 TNT
12 PETN
13 RDX
14 4-Amino-2,6-dinitrotoluene
15 3,5-Dinitroaniline
16 2-Amino-4,6-dinitrotoluene
17 Tetryl
18 HMX
Direct Injection
6m, 0.53mmID, 1.50µmRtx®-TNT (cat. #12998)
6m, 0.53mmID, 1.50µmRtx®-TNT2 (cat. #12999).
Direct injection using a 1mmSiltek™Uniliner®(cat. #21052-214.1).
On-column conc.: 200-1000pg for each compound. 8095Calibration
MixA(cat.#31607), 8095CalibrationMixB(cat.#31608), and 3,4-dinitrotoluene (cat.#31452).
Oven temp.: 80°C(hold1min.) to180°C@10°C/min. to300°C@30°C/min. (hold 3min.);
Inj. temp.: 250°C;Det.: ECD@330°Cwith anode purge;
Dead time: 4.4 sec.; Head pressure:
He@3psi (20.7KPa);
Flowrate: He@17mL/min.
@80°C.
