620
GC CHROMATOGRAMS |
FOODS, FLAVORS & FRAGRANCES
FAMEs
FAMEs (Marine Oil Standard)
FAMEWAX
GC_FF00568
1. C14:0
2. C15:0
3. C16:0
4. C16:1
5. C16:2
6. C17:0
7. C17:1
8. C16:4
9. C18:0
10. C18:1 (oleate)
11. C18:1 (vaccenate)
12. C18:2n6
cis
13. C18:3n3
14. C18:4n6
15. C18:4n3
16. C20:0
17. C20:1n7
18. C20:1n9
19. C20:4n6
20. C20:4n3
21. C20:5n3
22. C22:1n7
23. C21:5n3
24. C23:0 (IS)
25. C22:5n6
26. C22:5n3
27. C22:6n3
28. C24:1
Column:
FAMEWAX, 30m, 0.32mm ID, 0.25µm (cat.# 12498)
Sample:
12mg/mL total FAMEs
Inj.:
0.5µL, split (150:1), 3mm ID split liner for TRACE Series GCs, packed
with glass wool (cat.# 20936-202.1)
Inj. temp.:
250°C
Carrier gas:
hydrogen, constant flow
Linear velocity:
62cm/sec.
Oven temp.:
195°C to 240°C @ 5°C/min. (hold 1 min.)
Det.:
FID @ 250°C
FAST analysis!
Peak List
Conc. (µg/mL)
1. C14:0
600
2. C14:1
100
3. C16:0
1,600
4. C16:1
500
5. C18:0
800
6. C18:1 (oleate)
1,300
7. C18:1 (vaccenate)
400
8. C18:2
200
9. C18:3
200
10. C20:0
100
11. C20:1
900
12. C20:2
100
13. C20:4
300
14. C20:3
100
15. C20:5
1,000
16. C22:0
100
17. C22:1
300
18. C24:0
100
19. C22:6
1,200
20. C24:1
100
FAMEs (Marine Oil Standard)
FAMEWAX
Column:
FAMEWAX, 30m, 0.32mm ID, 0.25µm (cat.# 12498)
Inj.:
1µL
Conc.:
10,000µg/mL in isooctane (total FAMES; see breakdown in peak list)
Oven temp.:
195–240°C at 5°C/min., 1 min. hold
Inj./det. temp.:
250°C/275°C
Carrier gas:
hydrogen
Flow rate:
3mL/min. (constant flow)
Split ratio:
100:1
GC_FF00499
Column engineered
for optimal resolution.
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E-mail :
TelNo : 03 9762 2034 . . . in AUSTRALIA
Mar 2011
