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Exempted Drug of Abuse new!
Figure 1 Analyze acidi c drugs or basic drug s under t he same Reference Materials
cond itions, using an Rx( -Sms column. 1,0001lg/mL in P&T methanol (*exceptwhere noted),ImL/ampul
Acidic/neutral drugs
resolved to baseline
3 4 1.methprylon
2 2. butalbital
3. amobarbital
4. meprobamate
5. glutethimide
6. phenobarbital
7.methaqualone
8. primidone
GCPHOOS15
I
Sensitive analysis for
basic drugs in free base form
1. amphetamine
6 B
2. methamphetamine
3. nicotine
10 4. cotinine
5. caffeine
6. benzphetamine
7. ketamine
8. phencyclidine
9. methadone
10. cocaine
n . scopolamine
12. codeine
13. alprazolarn
13 12
11
Column:
Sample:
Inj.:
Ini, temp.:
Carrier gas:
Linear velocity:
Oven temp.:
Del.:
Transfer linetemp.:
Scanrange:
Tune:
Ionization:
Rxi'"-5ms30m, O,25mm!D, 0.25J.1m (cal.# 13423)
1000J.1g/ mLeach inmethanol
1.0J.1Lsplit (50:1), 20ng each compound oncolumn;
Siltek' treated 4mmgoosenecksplitless inlet liner (cat # 20799-214.5)
250'C
helium, constant pressure
30cm/sec.
100'C to 220'C@ 15' C/ min., to330'C @ 10°C/min. (hold5min.)
Agilent5973 MSD
300°C
35-550
PFTBA
EI
2006 vol. 1 • 9 •
Individual
_
Compound
Benzodiazepines
~razo lam 34042
bromazepam 34043
chlordiazepoxide HCL 34044
clobazam 34045
clonazepam 34046
diazepam 34047
flunitrazepam 34049
f1urazepam di-HCL 34050
loraze.l!!a1!.m!!.- 34051
""*~'i_----
nitrazepam 34053
oxaz~p)~a!!!mC_ __f;i*f.34054~----
prazepam 34055
34056 temazep@.a!!!m -:~~----
triazolam 34057
Cocaine &Metabolites
cocaine'..!C!'C",!,L'-,- 34015 ---- H --;;~c::___
34016 benzoy[ggjo!l!n!!!in.!.!'e'- ""*~!(------
ecgonine 34017
ecgonine methyl ester 34018
Methadone & Metabolites
methadone HCL 34005
Amphetamines & Metabolites
d-amphetamine 34020
{+)methamphetamine 34021
o iates& Metabolites
codeine 34000
h drocodone 34002
!)ydromorphone 34063
morphine 34006
oxycodone 34007
Oxymorphone 34065
cannabinoid & Metabolites
cannabidiol 34011
cannabinol 34010
Barbiturates!!- ---,;:;;;;;;n _
amobarbital 34028
~ roba rbital 34029
barbital 34030
butabarbital 34031
butalbital 34032
ii-glutethimide 34058
hexobarbital 34033
mephobarbital 34034
methohexital 34035
pentobarbital 34036
henobarbital
secobarbital
talbutal
34037
34038
34039
thiam,l!yl.2!al!,,34040--;;~~----
thiopental 34041
Other
benzphetamine
cocaethylene*
fenfluamine 34023
levorphanol 34003
meperidine 34004
meprobamate 34059
34064 methagualon!!'- ~~----_
methyprylon 34060
pentazocine 34062
phencyclidine 34027
phendimetrazine 34025
phenmetrazine 34026
phentermine 34024
dextro-propoxyphene 34008
thebaine 34009
Rxi™-Sms Column (fused silica) new!
(Crossbond' 5%diphenyl I 95%dimethylpolysiloxane)
10 df (um) temp. limits length cat.#
0.25mm 0.25 -60 to 330/350°C 30-Meter 13423
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