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15

800-356-1688 •

www.restek.com

2005 vol. 3

treated electropolished, electropolished, and standard tubing are compared in

Figure 1. Treated electropolished tubing reached the 98% saturation limit in

30 minutes, compared to 60 minutes for electropolished tubing. Standard tub-

ing could only achieve a 96% uptake, after 180 minutes.

After the tubing was stabilized with 1ppm of moisture, dry-down properties

were measured. Moisture dry-down curves for the three tubing treatments

show treated electropolished tubing achieved dry-down in 35 minutes, elec-

tropolished tubing required 65 minutes, and standard tubing required 175

minutes (Figure 2). Table 1 compares time to various dry-down levels for tub-

ing saturated with 10ppm of moisture.

Superior Corrosion Resistance: Silcosteel®-CR

In addition to rapid wet-up and dry-down, the other key advantage of Restek

treatment for 316L stainless steel is a dramatic improvement in corrosion

resistance. The amorphous silicon layer is insoluble in many acidic environ-

ments. Figures 3, 4, and 5 briefly summarize the results of corrosion testing by

ASTM methods. Comparisons between treated and untreated test samples

illustrate the improvements in corrosion resistance offered by Silcosteel®-CR

treatment. For more information about corrosion resistance, request infor-

mation packet 59048, or visit our website.

When moisture considerations and corrosion concerns arise in transfer of

ultra-high purity gas streams, Restek treated tubing and system components

will dramatically improve dry-down, reduce contamination from moisture

carryover, and extend periodic maintenance cycles.

Reference

1.

Relative Response Time of True Tube

when Measuring Moisture Content in a Sample Stream

Test Report,

Haritec Scientific & Engineering Support, Calgary, Alberta, Canada, May 2004.

Tubing used in the wet-up / dry-down experiments was supplied by Cardinal UHP (St. Louis, MO). All tubing was

tested as 100 foot coils of

1

/

4

" OD x 0.020" wall 316L stainless steel. Electropolished tubing had a surface rough-

ness of 10 to 15 microinches. Siltek

®

treated tubing was finished with 5µm of amorphous silicon, followed by a

surface functionalization to increase inertness and hydrophobicity.

Reference courtesy of O’Brien Corporation, available on request from Restek.

Silcosteel®-CR treated

untreated

Silcosteel®-CR treated

untreated

Figure 4

Silcosteel®-CR treated 316L

stainless steel shows no sign of attack after

4000-hour salt spray exposure (ASTM B117).

Figure 5

Silcosteel®-CR treated 316L

stainless steel shows no crevice corrosion

and only slight pitting corrosion after 72-

hour exposure to ferric chloride; untreated

steel exhibits severe crevice corrosion.

Siltek

®

Treated 316L Tubing**

Silcosteel

®

-CR -Treated 316L Tubing**

Silcosteel

®

-CR-Treated Electropolished Tubing

Siltek

®

-Treated Electropolished Tubing

Siltek®- and Silcosteel®-CR-Treated Electropolished Tubing

• Exceptional inertness.

• Improved reliability and reproducibility; longer lifetime.

• Use with treated fittings for the most inert sample pathway available.

1

/

8

" OD: 5 ft. to 100 ft. in one continuous coil;

1

/

4

" OD: 5 ft. to 300 ft. in one continuous coil.

Longer lengths will be more than one coil.

**0.035" wall thickness

Note: (required length in meters) x (3.2808) = length in feet.

Price-per-foot

ID

OD

cat.# 5-24 ft.

25-99 ft. 100-299 ft. >300 ft.

0.085"

1

/

8

"

22538

0.180"

1

/

4

"

22539

0.055" (1.40mm)

1

/

8

" (3.18mm)

22508

0.180" (4.57mm)

1

/

4

" (6.35mm)

22509

0.085"

1

/

8

"

22536

0.180"

1

/

4

"

22537

Price-per-foot

ID

OD

cat.# 5-24 ft.

25-199 ft. 200-399 ft. >400 ft.

0.055" (1.40mm)

1

/

8

" (3.18mm)

22896

0.180" (4.57mm)

1

/

4

" (6.35mm)

22897

Coiled, Treated, Seamless 316 Grade Stainless Steel Tubing

Figure 3

In chloride environments,

Silcosteel®-CR treated stainless steel

outperforms untreated metal by an order

of magnitude (ASTM G 48, Method B).

0

50

100

150 200 250

Untreated 316 SS

Silcosteel

®

-CR

weight loss in grams per square meter

for

more

info

Learn more about our precisely applied,

highly durable surface treatments:

www.restekcoatings.com