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www.restek.com2005 vol. 3
treated electropolished, electropolished, and standard tubing are compared in
Figure 1. Treated electropolished tubing reached the 98% saturation limit in
30 minutes, compared to 60 minutes for electropolished tubing. Standard tub-
ing could only achieve a 96% uptake, after 180 minutes.
After the tubing was stabilized with 1ppm of moisture, dry-down properties
were measured. Moisture dry-down curves for the three tubing treatments
show treated electropolished tubing achieved dry-down in 35 minutes, elec-
tropolished tubing required 65 minutes, and standard tubing required 175
minutes (Figure 2). Table 1 compares time to various dry-down levels for tub-
ing saturated with 10ppm of moisture.
Superior Corrosion Resistance: Silcosteel®-CR
In addition to rapid wet-up and dry-down, the other key advantage of Restek
treatment for 316L stainless steel is a dramatic improvement in corrosion
resistance. The amorphous silicon layer is insoluble in many acidic environ-
ments. Figures 3, 4, and 5 briefly summarize the results of corrosion testing by
ASTM methods. Comparisons between treated and untreated test samples
illustrate the improvements in corrosion resistance offered by Silcosteel®-CR
treatment. For more information about corrosion resistance, request infor-
mation packet 59048, or visit our website.
When moisture considerations and corrosion concerns arise in transfer of
ultra-high purity gas streams, Restek treated tubing and system components
will dramatically improve dry-down, reduce contamination from moisture
carryover, and extend periodic maintenance cycles.
Reference
1.
Relative Response Time of True Tube
™
when Measuring Moisture Content in a Sample Stream
Test Report,
Haritec Scientific & Engineering Support, Calgary, Alberta, Canada, May 2004.
Tubing used in the wet-up / dry-down experiments was supplied by Cardinal UHP (St. Louis, MO). All tubing was
tested as 100 foot coils of
1
/
4
" OD x 0.020" wall 316L stainless steel. Electropolished tubing had a surface rough-
ness of 10 to 15 microinches. Siltek
®
treated tubing was finished with 5µm of amorphous silicon, followed by a
surface functionalization to increase inertness and hydrophobicity.
Reference courtesy of O’Brien Corporation, available on request from Restek.
Silcosteel®-CR treated
untreated
Silcosteel®-CR treated
untreated
Figure 4
Silcosteel®-CR treated 316L
stainless steel shows no sign of attack after
4000-hour salt spray exposure (ASTM B117).
Figure 5
Silcosteel®-CR treated 316L
stainless steel shows no crevice corrosion
and only slight pitting corrosion after 72-
hour exposure to ferric chloride; untreated
steel exhibits severe crevice corrosion.
Siltek
®
Treated 316L Tubing**
Silcosteel
®
-CR -Treated 316L Tubing**
Silcosteel
®
-CR-Treated Electropolished Tubing
Siltek
®
-Treated Electropolished Tubing
Siltek®- and Silcosteel®-CR-Treated Electropolished Tubing
• Exceptional inertness.
• Improved reliability and reproducibility; longer lifetime.
• Use with treated fittings for the most inert sample pathway available.
1
/
8
" OD: 5 ft. to 100 ft. in one continuous coil;
1
/
4
" OD: 5 ft. to 300 ft. in one continuous coil.
Longer lengths will be more than one coil.
**0.035" wall thickness
Note: (required length in meters) x (3.2808) = length in feet.
Price-per-foot
ID
OD
cat.# 5-24 ft.
25-99 ft. 100-299 ft. >300 ft.
0.085"
1
/
8
"
22538
0.180"
1
/
4
"
22539
0.055" (1.40mm)
1
/
8
" (3.18mm)
22508
0.180" (4.57mm)
1
/
4
" (6.35mm)
22509
0.085"
1
/
8
"
22536
0.180"
1
/
4
"
22537
Price-per-foot
ID
OD
cat.# 5-24 ft.
25-199 ft. 200-399 ft. >400 ft.
0.055" (1.40mm)
1
/
8
" (3.18mm)
22896
0.180" (4.57mm)
1
/
4
" (6.35mm)
22897
Coiled, Treated, Seamless 316 Grade Stainless Steel Tubing
Figure 3
In chloride environments,
Silcosteel®-CR treated stainless steel
outperforms untreated metal by an order
of magnitude (ASTM G 48, Method B).
0
50
100
150 200 250
Untreated 316 SS
Silcosteel
®
-CR
weight loss in grams per square meter
for
more
info
Learn more about our precisely applied,
highly durable surface treatments:
www.restekcoatings.com