restekadv07 - page 182

• 9 •
800-356-1688
2,000µg/mL each inmethanol, 1mL/ampul
*(m- & p-xylene at 1,000µg/mL each)
Skinner List - Volatiles
(19 components)
benzene
2-butanone (MEK)
carbon disulfide
chlorobenzene
chloroform
1,2-dibromoethane (EDB)
1,1-dichloroethane
1,2-dichloroethane
1,4-dioxane
ethylbenzene
methyl
tert
-butyl ether (MTBE)
styrene
tetrachloroethylene
toluene
1,1,1-trichloroethane
trichloroethylene
m
-xylene*
o
-xylene
p
-xylene*
with data pack
Each
5-pk.
10-pk.
30491
30491-510
30491-500
30491-520
30591
2,000µg/mL each inmethylene chloride, 1mL/ampul
*(3- & 4-methylphenol at 1,000µg/mL each)
Skinner List - SV
(33 components)
with data pack
Each
5-pk.
10-pk.
31690
31690-510
31690-500
31690-520
31790
acenaphthene
anthracene
benzo(a)anthracene
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
bis(2-ethylhexyl)phthalate
(dioctylphthalate)
chrysene
dibenzo(a,h)acridine
dibenzo(a,h)anthracene
di-
n
-butylphthalate
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
diethylphthalate
2,4-dimethylphenol
dimethylphthalate
2,4-dinitrophenol
fluoranthene
fluorene
indene
indeno(1,2,3-cd)pyrene
1-methylnaphthalene
2-methylphenol (
o
-cresol)
3-methylphenol (
m
-cresol)*
4-methylphenol (
p
-cresol)*
naphthalene
4-nitrophenol
phenanthrene
phenol
pyrene
pyridine
quinoline
2,4-dinitrophenol
hexachlorocyclopentadiene
4-nitrophenol
N-nitroso-di-
n
-propylamine
2,000µg/mL each inmethylene chloride, 1mL/ampul
SV SystemPerformanceCheck
Mix (SPCC),
US EPAMethod 8270C/D
(4 components)
with data pack
Each
5-pk.
10-pk.
31689
31689-510
31689-500
31689-520
31789
OrganochlorinePesticideMixAB
#
3
(20 components)
2,000µg/mL each in hexane:toluene (1:1), 1mL/ampul
aldrin
α
-BHC
β
-BHC
δ
-BHC
γ
-BHC (lindane)
α
-chlordane
γ
-chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
dieldrin
endosulfan I
endosulfan II
endosulfan sulfate
endrin
endrin aldehyde
endrin ketone
heptachlor
heptachlor epoxide (isomer B)
methoxychlor
with data pack
Each
5-pk.
10-pk.
32415
32415-510
32415-500
32415-520
32515
PCBCongenerMix,Method 8082A
(19 components)
100µg/mL each in isooctane, 1mL/ampul
with data pack
Each
5-pk.
10-pk.
32416
32416-510
32416-500
32416-520
32516
2-chlorobiphenyl (BZ #1)
2,3-dichlorobiphenyl (BZ #5)
2,2',5-trichlorobiphenyl (BZ #18)
2,4',5-trichlorobiphenyl (BZ #31)
2,2',3,5'-tetrachlorobiphenyl (BZ #44)
2,2',5,5'-tetrachlorobiphenyl (BZ #52)
2,3',4,4'-tetrachlorobiphenyl (BZ #66)
2,2',3,4,5'-pentachlorobiphenyl (BZ #87)
2,2',4,5,5'-pentachlorobiphenyl (BZ #101)
2,3,3',4',6-pentachlorobiphenyl (BZ #110)
2,2',3,4,4',5'-hexachlorobiphenyl (BZ #138)
2,2',3,4,5,5'-hexachlorobiphenyl (BZ #141)
2,2',3,5,5',6-hexachlorobiphenyl (BZ #151)
2,2',4,4',5,5'-hexachlorobiphenyl (BZ #153)
2,2',3,3',4,4',5-heptachlorobiphenyl (BZ #170)
2,2',3,4,4',5,5'-heptachlorobiphenyl (BZ #180)
2,2',3,4,4',5',6-heptachlorobiphenyl (BZ #183)
2,2',3,4',5,5',6-heptachlorobiphenyl (BZ #187)
2,2',3,3',4,4',5,5',6-nonachlorobiphenyl (BZ #206)
Compound Conc. (%)
C4:0
1.5
C6:0
1.5
C8:0
2.0
C10:0
2.5
C11:0
2.5
C12:0
5.0
C13:0
2.5
C14:0
2.5
C14:1(
cis
-9)
1.5
C15:0
1.5
C16:0
10.0
C16:1(
cis
-9)
5.0
C17:0
2.5
C18:0
5.0
Compound Conc. (%)
C18:1(
trans
)
2.5
C18:1(
cis
)
15.0
C18:2(
trans
)
2.5
C18:2(
cis
)
10.0
C18:3
5.0
C20:0
2.5
C20:1
1.5
C20:5
2.5
C22:0
2.5
C22:1
1.5
C22:6
2.5
C23:0
1.5
C24:0
2.5
C24:1
2.5
NLEA FAMEMix
(28 components)
30mg/mL each inmethylene chloride, 1mL/ampul
ea.
35078
Compound
Conc. (%)
methyl elaidate (C18:1
trans
-9)
10.0
methyl linoleate (C18:2
cis
-9,12)
20.0
methyl oleate (C18:1
cis
-9)
10.0
methyl petroselinate (C18:1
cis
-6)
8.0
methyl petroselaidate (C18:1
trans
-6)
8.0
methyl stearate (C18:0)
20.0
methyl transvaccenate (C18:1
trans
-11)
12.0
methyl vaccenate (C18:1
cis
-11)
12.0
10mg/mL total inmethylene chloride, 1mL/ampul
cis
/
trans
FAMEMix
(8 components)
ea.
35079
GC_FF00652
Column:
Rt-2560, 100m, 0.25mm ID,
0.2µm (cat.# 13199)
Sample:
10mg/mL total FAMEs in
methylene chloride
Inj.:
1.0µL split (split ratio 20:1),
4mm inlet liner (cat.# 20814)
Inj. temp.:
225°C
Carrier gas:
hydrogen, constant flow
Flow rate:
1.2mL/min.
Oven temp.:
100°C (4min. hold)
to 240°C@ 3°C/min.
(10min. hold)
Det.:
FID@ 250°C
Compound
% inMix
1. C18:0 methyl stearate
20.0
2. C18:1methyl petroselaidate (
trans
-6)
8.0
3. C18:1methyl elaidate (
trans
-9)
10.0
4. C18:1methyl transvaccenate (
trans
-11) 12.0
5. C18:1methyl petroselinate (
cis
-6)
8.0
6. C18:1methyl oleate (
cis
-9)
10.0
7. C18:1methyl vaccenate (
cis
-11)
12.0
8. C18:2methyl linoleate (
cis
-9,12)
20.0
See page 11
for more
information on
FAME analysis
What’sNew inThis Issue
Skinner Semivolatiles&VOAs, Chlorinated Pesticides, PCBs, FAMEs
• Use as a calibration standard for AOAC
Method 996.06.
• Use to identify the isomers of octadecenoic acid.
1...,172,173,174,175,176,177,178,179,180,181 183,184,185,186,187,188,189,190,191,192,...297
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