fastfacts07 - page 63

800-356-1688
814-353-1300
At-a-Glance
Product
Information
fromRestek
JoeMoodler
Analytical ReferenceMaterials
CustomStandards Group Leader
814-353-1300, ext. 2148
Ken Herwehe
Analytical ReferenceMaterials
Product MarketingManager
814-353-1300, ext. 2127
For
complete lists
of standards, columns
and current prices, visit our website at:
Lit. Cat. #59383A
Calibration Standards
for ASTMMethod D2887-01,
Boiling Range Distribution
of PetroleumProducts
American Society for Testing and Materials (ASTM International) Method D2887-01,
Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas
Chromatography,
describes the determination of the boiling range distribution of petrole-
um products. This test method is applicable to petroleum products and fractions having a
final boiling point of 538°C (1000°F) or lower; and is limited to samples having a boiling
range greater than 55°C (100°F) and having a vapor pressure sufficiently low to permit
sampling at ambient temperature.
To facilitate the ASTM International guideline and help petroleum analytical laboratories in
determiningpetroleumproduct boiling range applications, Restekhas introduced two chemical
standardsdesignedspecificallyforASTMMethodD2887-01.Thefirstmixture ispreparedat1%
w/w in carbon disulfide for convenient laboratory use. This standardmay only be shipped by
ground shipment within theUS. The secondmixture is a blend of neat hydrocarbons to allow
overnight shipments in theUS and shipments toour international customers.
This method is not to be used for the analysis of gasoline samples or gasoline range
petroleum products. These types of samples must be analyzed by ASTM Method
D3710-95. Restek offers a calibrationmixture forASTMD-3710-95. (cat.# 31223, single
ampul, and cat.# 31323, 10-packwith data pack)
In addition, Restek offers chemical standards for other ASTM Methods: D6352-98
(Polywax
®
); E1387-95 and E1618-97 (fire debris); and D-4059-96 (PCBs in transformer
oil). Restek also makes custom chemical standard solutions for a wide variety of ASTM
Methods— see the reverse side of this
Fast Facts
for information.
Capillary GCColumns for ASTMD-2887-01
Rtx
®
-2887 10m x 0.53mm x 2.65µm (cat.# 10199)
MXT
®
-2887 10m x 0.53mm x 2.65µm (cat.# 70199)
Meet requirements for the 2001 revision of ASTM 2887-01.
Pentane added.
Equal weight/weight concentrations of all components.
Designed for both calibration and resolution tests—
one sample for both test criteria.
ASTMD2887-01 HydrocarbonMixture in Carbon Disulfide
1%w/w each component in carbon disulfide, 1mL/ampul
cat.#/Each
5-pk.
10-pk.
31674
31674-510
w/data pack
31674-500
31674-520
31774
Solvent-Free ASTMD2887-01 HydrocarbonMixture
5%w/w each component*, 1g/5mL ampul
cat.#/Each
5-pk.
10-pk.
31675
31675-510
w/data pack
31675-500
31675-520
31775
*Thismixturemay be diluted by the analyst with 4g carbon disulfide to achieve a concentration of 1%w/w.
Components of ASTMD2887-01
HydrocarbonMixtures
n
-pentane
(C5)
n
-hexane
(C6)
n
-heptane
(C7)
n
-octane
(C8)
n
-nonane
(C9)
n
-decane
(C10)
n
-undecane (C11)
n
-dodecane (C12)
n
-tetradecane (C14)
n
-pentadecane (C15)
n
-hexadecane (C16)
n
-heptadecane (C17)
n
-octadecane (C18)
n
-eicosane
(C20)
n
-tetracosane (C24)
n
-octacosane (C28)
n
-dotriacontane (C32)
n
-hexatriacontane(C36)
n
-tetracontane (C40)
n
-tetratetracontane(C44)
12
s
p
e
t
s
Separating Restek from
the rest through
12 critical steps.
1. Reviewmethod requirements
2. Verify compatibility and stability
3. Test startingmaterials
4. Certify balance andweights
5. Deactivate glassware and ampuls
6. Prepare two independent lots
7. Assay to assure quality
8. Assign real-time expiration date
9. Use customer friendly packaging
(includes extra vial and label)
10. IncludeRestek documentation
11. Complywith ISO 9001 registration
12. Offer custom referencematerials program
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