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www.restekcorp.com

Stx

®

-1HT Columns

cont.

30m, 0.32mm ID, 0.10µm Stx

-1HT (cat.# 11709); 0.20µL injection of D2887 calibration mix

(cat.# 31222), plus C46 to C58 hydrocarbons;

Solvent:

carbon disulfide;

GC:

Agilent 6890;

Oven program:

30°C to

380°C at 10°C/min. (hold 15 min.);

Detector:

FID @ 380°C;

Injector:

cool on-column/track oven temperature;

Carrier gas:

helium;

Flow rate:

1.3cc/min. @30°C;

Linear velocity:

22cm/sec. @ 30°C, constant pressure with EPC;

Make-up gas flow:

45cc/min.;

Head pressure:

6.0psi

min.

10

20

30

40

50

1

2

3

4

5

6

7

8

9

10 11

12 13 14 15 16 17 18 19 20 21 22 23

1. C7

2. C8

3. C9

4. C10

5. C11

6. C12

7. C14

8. C16

9. C18

10. C20

11. C24

12. C28

13. C32

14. C36

15. C40

16. C44

17. C46

18. C48

19. C50

20. C52

21. C54

22. C56

23. C58

<10pa at

380°C!

Figure 2

The Stx

-1HT column is an excellent choice for high-temperature, low-bleed

hydrocarbon analysis up to C58.

Stx

®

-1HT Columns

(100% dimethylpolysiloxane) Stable to 380°C

ID

df (µm)

temp. limits

15-Meter

30-Meter

0.25mm

0.10

-60 to 380°C

11705

11708

0.32mm

0.10

-60 to 380°C

11706

11709

rules, high-temperature septa, and checking con-

nectors for leaks after every thermal cycle.

Stringent quality assurance specifications ensure

consistent column-to-column reproducibility for

Stx

®

-1HT columns. Each column is tested for inert-

ness, efficiency, and bleed level at its maximum

temperature (380°C). In fact, Stx

®

-1HT columns

are guaranteed to exhibit less than 10pA of bleed at

380°C in a leak-free system.

The Stx

®

-1HT column is a major advancement for

high-temperature analysis. The combination of

Siltek

deactivation, high-temperature fused silica

tubing, and a specially synthesized stationary phase

has created a column that exhibits low bleed at

temperatures as high as 380°C.

A long-standing customer of Restek received his column only to find it was

mangled by postal machinery. Fearful of what he might find inside, he was

relieved when the column’s tubing was still intact! He supplied these pic-

tures to illustrate the endurance of Restek’s strong column cage.

Do you have a similar story to share? Tell us about it by calling 800-356-

1688 or 814-353-1300, ext. 4, or contact your local Restek representative.

Restek Columns Are Tough!

Strong Cage Helps Column Survive Rough Journey

D2887 SimDist Calibration Mix

Compound

Conc.

Compound

Conc.

(% w/w)

(% w/w)

n

-hexane (C6)

6

n

-octadecane (C18)

5

n

-heptane (C7)

6

n

-eicosane (C20)

2

n

-octane (C8)

8

n

-tetracosane (C24)

2

n

-nonane (C9)

8

n

-octacosane (C28)

1

n

-decane (C10)

12

n

-dotriacontane (C32)

1

n

-undecane (C11)

12

n

-hexatriacontane (C36)

1

n

-dodecane (C12)

12

n

-tetracontane (C40)

1

n

-tetradecane (C14) 12

n

-tetratetracontane (C44)

1

n

-hexadecane (C16) 10

Packaged 1mL per ampul

Ea.

10-pk.w/data pack

31222

31322

Siltek

Guard Colums

ID Nominal OD 5-Meter

10-Meter

0.25mm 0.37 ±0.04mm 10026

10036

0.32mm 0.45 ±0.04mm 10027

10037

Siltek

Inlet Liners

Add the appropriate suffix to your Restek liner catalog number.

For a complete inlet liner offering, refer to the

Restek Annual Chromatography Products Guide

(lit. cat.# 59960).

qty.

Siltek

Siltek

with Siltek

wool

Siltek

with CarboFrit

each

-214.1 addl. cost

-213.1 addl. cost

-216.1 addl. cost

5-pack

-214.5 addl. cost

-213.5 addl. cost

-216.5 addl. cost

25-pack

-214.25 addl. cost

-213.25

addl. cost

-216.25

addl. cost

Siltek

Press-Tight

®

Connectors

Type

5-pk.

25-pk.

100-pk.

straight

20480

20449

20481

angled 20482

20483

20484

Thermolite

®

Septa

Diameter 25-pk.

50-pk.

100-pk.

5mm 20351

20352

20353

9.5mm 20359

20360

20361

10mm 20378

20379

20380

11mm 20363

20364

20365

11.5mm 22385

22386

22387

17mm 20384

20385

20386

Plug

20372

20373

20374

GC_PC00378

for

more

info

request the “Stx

®

-1HT Benefits Brochure”

(lit. cat.# #59283).