Capillary
Nut
$175
22423
kit
EZ No-Vent
™
Connector Kit for Varian Saturn 2000 Series MSs
• 23 •
800-356-1688 •
www.restek.com2005 vol. 1
EZ No-Vent™ GC Column-MS Connector
Change Columns in Minutes Without Venting
by Donna Lidgett, GC Accessories Product Marketing Manager
•Save hours of downtime—100µm transfer line throttles vacuum and prevents MS pump-
down.
• Easy to install and maintain—no special tools or plumbing required.
•Gold-plated body for inertness.
•Deactivated transfer line keeps analytes focused; high-temperature polyimide ferrules
eliminate leaks at the problematic transfer line fitting.
• Lower cost than other “no-vent” fittings.
•Available for Agilent GCs with 5971/5972 or 5973 GC/MS, Varian Saturn 2000 Series MSs.
We designed the EZ No-Vent
™
connector to be
simple and easy to use. A critical orifice in
the EZ No-Vent
™
connector minimizes the
amount of oxygen allowed into the MS
source, eliminating the need for purge gas
and enabling you to skip the lengthy vent and
pump-down cycle otherwise required when
you make a column change. This can save
nearly a day of downtime with each column
change. The EZ No-Vent
™
connector easily
attaches to the MS source without special
tools or extra plumbing.
Description
qty.
cat.#
price
EZ No-Vent
™
Connector Kit for Agilent 5971/5972 and 5973 GC/MS
kit
21323
$175
Replacement ferrules for connecting capillary column to EZ No-Vent
™
:
0.4mm ID
2-pk.
21015
$28
0.5mm ID
2-pk.
21016
$28
Replacement ferrules for connecting transfer line to EZ No-Vent
™
: 0.4mm ID
2-pk.
21043
$25
Replacement 100µm deactivated transfer line
3 ft.
21018
$20
Replacement EZ No-Vent
™
Column Nut
5-pk.
21900
$30
Replacement EZ No-Vent
™
Plug
2-pk.
21915
$36
Open-End Wrenches (
1
/
4
" x
5
/
16
")
2-pk.
20110
$25
3.5 3.7 3.9 4.1 4.3 4.5 4.7 4.9 5.1 5.3 5.5
min.
2
1
3
4
5
6
7
3.5 3.7 3.9 4.1 4.3 4.5 4.7 4.9 5.1 5.3 5.5
min.
4
5
6
1
2
3
7
502.2 Calibration Mix#1 (gases) cat# 30042
1. dichlorodifluoromethane
2. 1,2-dichlorotetrafluoroethene (Freon
®
114)
3. chloromethane
4. vinyl chloride
5. bromomethane
6. chloroethane
7. trichlorofluoromethane
Column:
Rtx
®
-624 60m, 0.25mm ID, 1.4µm (cat# 10969)
Inj.:
purge & trap
GC
Agilent 6890
Inj. temp.:
300°C
Carrier gas:
helium, constant flow
Flow rate:
1.0mL/min.
Oven temp.:
60°C
Det:
Agilent 5973 GC/MS
Transfer line temp.: 280°C
Scan range:
35-550 amu
Tune
BFB
Ionization:
EI
GC_EV00659a
GC_EV00659b
Figure 2
Sharp, symmetric peaks for gases show the EZ No-Vent™ connector does not add dead volume and allows rapid column changes.
1st column, equilibrated system
Acquired 76 minutes after installing
2nd column, using EZ No-Vent™
GC/MS
Interface
Transfer
Line
Ferrule
EZ No-Vent
™
Connector
Capillary
Ferrule
Capillary
Column
Transfer
Line
Figure 1
A laser machined
orifice, coupled with the
100µm ID transfer line,
minimizes the amount of
oxygen entering the MS,
which eliminates the need
for purge gases.
Laser drilled to
100µm ID
did you
know
?
Restek offers many innovative
tools and supplies for your
MS. Refer to our catalog or
website.
new
!
Each kit includes: EZ No-Vent
™
Connector, two 0.4mm ID ferrules for
capillary column, two 0.4mm ID ferrules
for transfer line, 100µm deactivated
transfer line (3 ft.), column plug, column
nut.
new
!
Now available for Varian 2000 Series MSs