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Capillary

Nut

$175

22423

kit

EZ No-Vent

Connector Kit for Varian Saturn 2000 Series MSs

• 23 •

800-356-1688 •

www.restek.com

2005 vol. 1

EZ No-Vent™ GC Column-MS Connector

Change Columns in Minutes Without Venting

by Donna Lidgett, GC Accessories Product Marketing Manager

•Save hours of downtime—100µm transfer line throttles vacuum and prevents MS pump-

down.

• Easy to install and maintain—no special tools or plumbing required.

•Gold-plated body for inertness.

•Deactivated transfer line keeps analytes focused; high-temperature polyimide ferrules

eliminate leaks at the problematic transfer line fitting.

• Lower cost than other “no-vent” fittings.

•Available for Agilent GCs with 5971/5972 or 5973 GC/MS, Varian Saturn 2000 Series MSs.

We designed the EZ No-Vent

connector to be

simple and easy to use. A critical orifice in

the EZ No-Vent

connector minimizes the

amount of oxygen allowed into the MS

source, eliminating the need for purge gas

and enabling you to skip the lengthy vent and

pump-down cycle otherwise required when

you make a column change. This can save

nearly a day of downtime with each column

change. The EZ No-Vent

connector easily

attaches to the MS source without special

tools or extra plumbing.

Description

qty.

cat.#

price

EZ No-Vent

Connector Kit for Agilent 5971/5972 and 5973 GC/MS

kit

21323

$175

Replacement ferrules for connecting capillary column to EZ No-Vent

:

0.4mm ID

2-pk.

21015

$28

0.5mm ID

2-pk.

21016

$28

Replacement ferrules for connecting transfer line to EZ No-Vent

: 0.4mm ID

2-pk.

21043

$25

Replacement 100µm deactivated transfer line

3 ft.

21018

$20

Replacement EZ No-Vent

Column Nut

5-pk.

21900

$30

Replacement EZ No-Vent

Plug

2-pk.

21915

$36

Open-End Wrenches (

1

/

4

" x

5

/

16

")

2-pk.

20110

$25

3.5 3.7 3.9 4.1 4.3 4.5 4.7 4.9 5.1 5.3 5.5

min.

2

1

3

4

5

6

7

3.5 3.7 3.9 4.1 4.3 4.5 4.7 4.9 5.1 5.3 5.5

min.

4

5

6

1

2

3

7

502.2 Calibration Mix#1 (gases) cat# 30042

1. dichlorodifluoromethane

2. 1,2-dichlorotetrafluoroethene (Freon

®

114)

3. chloromethane

4. vinyl chloride

5. bromomethane

6. chloroethane

7. trichlorofluoromethane

Column:

Rtx

®

-624 60m, 0.25mm ID, 1.4µm (cat# 10969)

Inj.:

purge & trap

GC

Agilent 6890

Inj. temp.:

300°C

Carrier gas:

helium, constant flow

Flow rate:

1.0mL/min.

Oven temp.:

60°C

Det:

Agilent 5973 GC/MS

Transfer line temp.: 280°C

Scan range:

35-550 amu

Tune

BFB

Ionization:

EI

GC_EV00659a

GC_EV00659b

Figure 2

Sharp, symmetric peaks for gases show the EZ No-Vent™ connector does not add dead volume and allows rapid column changes.

1st column, equilibrated system

Acquired 76 minutes after installing

2nd column, using EZ No-Vent™

GC/MS

Interface

Transfer

Line

Ferrule

EZ No-Vent

Connector

Capillary

Ferrule

Capillary

Column

Transfer

Line

Figure 1

A laser machined

orifice, coupled with the

100µm ID transfer line,

minimizes the amount of

oxygen entering the MS,

which eliminates the need

for purge gases.

Laser drilled to

100µm ID

did you

know

?

Restek offers many innovative

tools and supplies for your

MS. Refer to our catalog or

website.

new

!

Each kit includes: EZ No-Vent

Connector, two 0.4mm ID ferrules for

capillary column, two 0.4mm ID ferrules

for transfer line, 100µm deactivated

transfer line (3 ft.), column plug, column

nut.

new

!

Now available for Varian 2000 Series MSs