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mix components. Over the course of the study, the
variation in the peak retention times was 0.08-
0.22% RSD. This includes the polar free fatty acids,
which can be difficult to analyze under ideal condi-
tions. The excellent stability of this stationary phase
is proven by the reproducibility of the retention
times over the course of the water stability study.
The Stabilwax
®
-DA column is an excellent choice
for the analysis of acids, esters, and other flavor
components in alcoholic beverage products. This
highly stable column has been optimized for the
analysis of acidic compounds, making it possible to
analyze a wide range of compounds in a single
injection. In addition, the column configuration
shown in this article allows fast, efficient separation
of the test compounds.
0
2
4
6
8
10
12
14
16
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
Figure 3
Excellent stability and peak shapes for free fatty acids after fifty 1µL splitless
injections of water demonstrates column ruggedness and long lifetime.
30m, 0.18mm ID, 0.18µm
Stabilwax
®
-DA (cat.# 5550752)
Oven temp.:
70 to 240°C at
12°C/min. (hold 3 min.);
See Figure 1 for complete
conditions and peak list.
Ethanol Standards
All standards are available in a 5-ampul minimum purchase.
Expiration date for each solution is 36 months from the date of manufacture.
concentration
cat.#
minimum purchase of 5 ampuls
25mg/dL in water
550741
40mg/dL in water
550742
100mg/dL in water
550743
150mg/dL in water
550744
200mg/dL in water
550745
300mg/dL in water
550746
by Ken Herwehe, Analytical Reference Materials Product Marketing Manager
Ethanol Analytical
Reference Materials
For Blood Alcohol Testing
✔
Resolution control standard for calibration of whole analytical system.
✔
Custom mixes for 6-point calibration of your instrument.
✔
Confidence ensured with a Certificate of Analysis, raw materials test
results, statistical QA results, analytical balance printout, and a lot
sheet showing gravimetric weight of each analyte.
Resolution Control Standard
The ethanol concentration will be a certified value.
The concentration of the other analytes will be
reported as gravimetric concentration only.
Expiration date is 18 months from the date of
manufacture.
Contains:
ethanol
methyl ethyl ketone
methanol
acetaldehyde
isopropanol
acetonitrile
acetone
ethyl acetate
concentration
cat.#
100mg/dL each compound in water
550778
minimum purchase of 10 ampuls
Stabilwax
®
-DA Columns
ID (mm)
df (µm)
temp. limits
15-Meter
30-Meter
60-Meter
0.18
0.18
40 to 250°C
—
—
0.25
0.10
40 to 250°C
0.25
40 to 250°C
0.50
40 to 250°C
0.32
0.10
40 to 250°C
0.25
40 to 250°C
0.50
40 to 250°C
1.00
40 to 240/250°C
0.53
0.10
40 to 250°C
0.25
40 to 250°C
0.50
40 to 250°C
1.00
40 to 240/250°C
1.50
40 to 230/240°C
for
more
info
request the Stabilwax
®
/MXT
®
-WAX Fast
Facts flyer (lit. cat.# #59316).
GC_FF00526
min.
4mm Splitless Inlet Liner for
ThermoQuest Trace GCs
4.0mm ID, 5.5mm OD, 79.5mm length
Add suffix -202.1 for wool packing.
each
5-pk.
25-pk.
Rtx
®
-BAC1 Columns
Temp. limits: -20 to 240/260°C
ID
df (µm)
30-Meter
0.32mm
1.80
0.53mm
3.00
Rtx
®
-BAC2 Columns
Temp. limits: -20 to 240/260°C
ID
df (µm)
30-Meter
0.32mm
1.20
0.53mm
2.00
for
more
info
request the Application Note
Dual-Column Confirmational GC Analysis of Blood Alcohols Using the
Rtx
®
-BAC1 and Rtx
®
-BAC2 Columns
(lit. cat.# #59598).
20816
20815
20814
11011
11008
11005
550752
11020
11023
11026
11038
11041
11035
11009
11012
11006
11024
11021
11027
11039
11036
11042
11054
11051
11057
11010
11007
11013
11025
11022
11028
11040
11037
11043
11055
11052
11058
11065
11062
11068
10 x 1mL ampuls
18003
18002
18001
18000
5 x 20mL ampuls
5 x 20mL ampuls
5 x 20mL ampuls
5 x 20mL ampuls
5 x 20mL ampuls
5 x 20mL ampuls