678
GCCHROMATOGRAMS |
FORENSIC/PHARMACEUTICAL
Barbiturates
6 7 5
Column:
Rtx
®
-35, 30m, 0.53mm ID, 1.0µm (cat.# 10455)
Sample:
1.0µL splitless injection of acidic/neutral drugs
Conc.:
50µg/mL
Oven temp.:
100°C to 280°C@ 10°C/min. (hold 5min.)
Inj./det. temp.:
250°C
Carrier gas:
helium
Linear velocity:
40cm/sec. set@ 100°C
FID sensitivity:
5.12 x 10
-10
AFS
Splitless hold time: 0.5min.
Barbiturates (Acidic/NeutralDrugs) (Underivatized)
Rtx®-35
1
2
3
4
8
9
11
10
12
13
16
15
14
min.
0
5
10
15
20
GC_PH00262
1. ethosuximide
2. barbital
3. methyprylon
4. aprobarbital
5. butalbital
6. amobarbital
7. pentobarbital
8. secobarbital
9. meprobamate
10. carisoprodal
11. glutethimide
12. phenobarbital
13. methaqualone
14. primidone
15. carbamazepine
16. diphenylhydantoin
Column:
Rtx
®
-1701, 15m, 0.53mm ID, 0.50µm (cat.# 12037)
Sample:
1.0µL splitless injection of acidic/neutral drugs
Conc.:
50µg/mL concentration
Oven temp.:
100°C to 280°C@ 7°C/min.
Inj./det. temp.:
250°C/275°C
Carrier gas:
helium
Linear velocity:
40cm/sec. set@ 100°C
FID sensitivity:
5.12 x 10
-10
AFS
Splitless hold time: 0.5min.
6 7
Barbiturates (Acidic/NeutralDrugs) (Underivatized)
Rtx®-1701
1
3
2
4
5
8
11
9
15
10
12
13
14
16
min.
0
5
10
15
20
GC_PH00263
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E-mail :
TelNo : 03 9762 2034 . . . inAUSTRALIA
Mar 2011
