SympathomimeticAmines (BasicDrugs) (Underivatized)
Rtx®-5Amine
1
2
3
4
5
6
7 8
9
10
11,12
13
14
15
16
17
18
19
21
22
1. phenylethylamine
2. amphetamine
3. phentermine
4. methamphetamine
5. fenfluramine
6. mephentermine
7. cathinone
8. phenylpropanolamine
9. methcathinone
10. nicotine
11. ephedrine
12. pseudoephedrine
13. phenmetrazine
14. phendimetrazine
15. methylenedioxyamphetamine
16. diethylpropion
17. methylenedioxymethamphetamine
18. methylenedioxyethylamphetamine
19. 4-methyl-2,5-dimethoxyamphetamine
20. phenylephrine
21. caffeine
22. benzphetamine
Column:
Rtx
®
-5 Amine, 30m, 0.25mm ID, 0.50µm (cat.# 12338)
Instrument:
Varian 3400GC coupledwith Varian Saturn 2000MS detector
Inj.:
1µL, split, split vent flow rate 45mL/min.
Inj. temp.:
250°C
Carrier gas:
helium
Det.:
mass spectroscopy data collected using a scan range of 40 amu through 600 amu.
Oven temp.:
100°C to 310°C@ 10°C/min.
Ionization performed in the EI Automode.
min.
5
7.5
10
12.5
15
17.5
20
GC_PH00438
SympathomimeticAmines (BasicDrugs) (HFBADerivatized)
Rtx®-200
min.
5
7.5
10
12.5
15
17.5
10
14
3
1,2
16
4
8
11
9
7
5
12
13
22
15,20
19 17
18
21
Column:
Rtx
®
-200, 30m, 0.25mm ID, 0.50µm (cat.# 15038)
Instrument:
Varian 3400GC coupledwith Varian Saturn 2000MS detector
Inj.:
1µL, split, split vent flow rate 45mL/min.
Inj. temp.:
250°C
Carrier gas:
helium
Det.:
mass spectroscopy data collected using a scan range of 40 amu through 600 amu.
Oven temp.:
100°C to 310°C@ 10°C/min.
Ionization performed in the EI Automode.
GC_PH00439
676
GCCHROMATOGRAMS |
FORENSIC/PHARMACEUTICAL
Sympathomimetic Amines
Website :
E-mail :
TelNo : 03 9762 2034 . . . inAUSTRALIA
Mar 2011
