531
REFERENCESTANDARDS |
FOODS, FLAVORS&FRAGRANCESMATERIALS
Flavors & Fragrances, Nutritional Analysis
OrganicacidsonanAllure®OrganicAcidsHPLC
column.
Flavors
citric acid
2,000µg/ml
fumaric acid
10*
malic acid
2,000
quinic acid
2,000
tartaric acid
2,000
Fruit JuiceOrganicAcidStandard
(5 components)
Inwater, 1mL/ampul
cat.# 35080 (ea.)
Inwater, 5mL/ampul
cat.# 35081 (ea.)
Peak List:
Conc. (mg/mL)
1. tartaric acid
1
2. quinic acid
1
3. malic acid
1
4. citric acid
1
5. fumaric acid
0.005
Sample:
Inj.:
10µL standard solution
Solvent:
water
Column:
Allure
®
Organic Acids
Cat.#:
9165585
Dimensions:
300mm x 4.6mm
Particle size:
5µm
Pore size:
60Å
Conditions:
Mobile phase:
100mM phosphate buffer, pH 2.5
Flow:
0.5mL/min.
Temp.:
ambient
Det.:
UV@ 226nm
LC_0238
*Fumaric acid is a trace impurity inmalic acid, aswell as an added component
of themix.The amount of fumaric acid inmalic acidwill not affect the stated
concentration of malic acid, but can represent a significant and variable devia-
tion from the low concentration of fumaric acid stated to be in themix. All other
components of themix are at the specified concentration.
Quantity discounts not available.
FattyAcidMethyl Esters (FAMEs)
Chain Description
% byWeight
C14:0 methyl myristate
6.0
C14:1 methyl myristoleate
1.0
C16:0 methyl palmitate
16.0
C16:1 methyl palmitoleate
5.0
C18:0 methyl stearate
8.0
C18:1 methyl oleate
13.0
C18:1 methyl vaccenate
4.0
C18:2 methyl linoleate
2.0
C18:3 methyl linolenate
2.0
C20:0 methyl arachidate
1.0
C20:1 methyl 11-eicosenoate
9.0
C20:2 methyl 11-14-eicosadienoate
1.0
C20:4 methyl arachidonate
3.0
C20:3 methyl 11-14-17-eicosatrienoate
1.0
C20:5 methyl eicosapentaenoate
10.0
C22:0 methyl behenate
1.0
C22:1 methyl erucate
3.0
C22:6 methyl docosahexaenoate
12.0
C24:0 methyl lingnocerate
1.0
C24:1 methyl nervonate
1.0
MarineOilFAMEMix
(20 components)
cat.# 35066 (100mg)
Description
% byWeight
methyl elaidate (C18:1
trans
-9)
10.0
methyl linoleate (C18:2
cis
-9,12)
20.0
methyl oleate (C18:1
cis
-9)
10.0
methyl petroselinate (C18:1
cis
-6)
8.0
methyl petroselaidate (C18:1
trans
-6)
8.0
methyl stearate (C18:0)
20.0
methyl transvaccenate (C18:1
trans
-11)
12.0
methyl vaccenate (C18:1
cis
-11)
12.0
cis
/
trans
FAMEMix
(8 components)
10mg/mL total inmethylene chloride, 1mL/ampul
cat.# 35079 (ea.)
No data pack available.
Quantity discounts not available.
No data pack available.
Quantity discounts not available.
acetic acid
butyric acid (C4:0)
isobutyric acid
isovaleric acid
propionic acid
valeric acid
FreeFattyAcidsTestStandard
(6 components)
1,000µg/mL each inwater, 1mL/ampul
cat.# 35272 (ea.)
StandardMethods for theExaminationofWater and
WastewaterMethod5560:OrganicandVolatileAcids
Themeasurementof organicacids, eitherbyadsorptionandelu-
tion from a chromatographic column or by distillation, can be
used as a control test for anaerobic digestion. The chromato-
graphic separation method is presented for organic acids
(5560B), while amethodusing distillation (5560C) is presented
for volatile acids. A newmethod using gas chromatography is
included for the determination of acetic, propionic, butyric,
isobutyric, valeric, and isovaleric acids (5560D).
benzoic acid
1.0%
benzyl salicylate
36.2%
1,8-cineole (eucalyptol)
0.5%
trans
cinnamaldehyde
0.5%
cinnamyl acetate
0.3%
cinnamyl alcohol
0.3%
ethyl butyrate
36.2%
geraniol
0.6%
hydroxycitronellal (3,7-dimethyl-
7-hydroxyoctanal)
5.0%
d-limonene
20.0%
thymol
0.3%
vanillin
0.1%
FragranceMaterialsTestMix
(12 components)
TheFragranceMaterialsAssociation (FMA)hasproposedamethod
for analyzing essential oils on polar and nonpolar capillary GC
columns.Aperformanceevaluationmixtureshouldbeused toaid in
detecting inlet problems, stationaryphasedegradation, loss of reso-
lution, changes in sensitivity, and thepresenceof reactive sites in the
sample pathway. Our test mix is consistent with the mixture pro-
posedby the FMA.The required 5% test solution ismade bydilut-
ing the 0.5mLof neatmixture to 10mLwith acetone. Theworking
solution will be stable for up to one week if transferred to a dark
container and stored refrigerated.
Neat, 0.5mL in an amber ampul
cat.# 31807 (ea.)
No data pack available.
Quantity discounts not available.
Fragrances
Website :
E-mail :
TelNo : 03 9762 2034 . . . inAUSTRALIA
Mar 2011
