SRITN12 - page 291

Expected Performance
Thesetwonoiserunsweremadewithidenticalparameters(carrierflow,columns,temperatureprogram)
onaMultipleGasAnalyzer#2GCequippedwithFIDandTCDdetectors. Theonlydifferencesare the
detectorparticulars,whichare listednext to theappropriatechromatogram.
FIDnoise run
FIDgain=HIGH
FID temp=380
o
C
FID ignitor= -400
Methanizer inFID
detector body
Temperatureprogram:
Initial
Hold Ramp Final
80
o
C 20.00 0.00 80
o
C
Valve temp=90
o
C
Carrier#1Mol.Sieve13x=20mL/min
Carrier#2Hayesep-D=20ml/min
Total carrier flow=40mL/min
TCDnoise run
TCDcurrent=LOW
TCD temp=150
o
C
POPULAR CONFIGURATION GCs
Multiple Gas Analyzer #2
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