Chromatography Columns 2013+ - page 342

Lit. Cat.#580147
© 2007 Restek Corporation.
1.9μmPinnacle™DBC18HPLCColumns
Restek’spopularPinnacle™DBHPLCcolumnsare
nowavailable ina<2μmparticlesize.
Ruggedness and reproducibility are guaranteed, as we
control every step in the process, from base silica to
bonded phase to final packed column. The silica parti-
cles are classified and selected to give an exceptionally
tight distribution around 1.9µm, while eliminating
<1µm particles that can contribute to a poorly packed
bed. Highly base-deactivated Pinnacle™DB stationary
phases are an excellent choice when analyzing a wide
range of compounds, from acidic to basic. To optimize
your ultra high pressure HPLC methods, reach for
Restek small particleHPLC columns!
Figure1
—Pinnacle™DB silicaparticle sizedistribution chart shows anexceptionally
tight, symmetrical distributionaround1.9μmwithno<1μmparticles.
RestekTrademarks: Pinnacle, Restek logo.
1.9μmPinnacle™DBC18HPLCColumns
ChromatographicProperties:
Highlybase-deactivated spherical silicamanufacturedby
Restek.MonomericC18bonding.
particle size: 1.9µm
pore size: 140Å
carbon load: 11%
endcap: yes
pH range: 2.5 - 10
temperature limit: 80°C
PhysicalCharacteristics:
2.1mm ID
Length
cat.#
price
1.9µmColumns
30mm
9414232
$440
50mm
9414252
$460
100mm
9414212
$520
Sample:
Inj.:
2µL
Sample diluent: water:methanol (25:75)
Sample temp.: ambient
Column:
Pinnacle
DBC18
Cat.#:
9414252
Dimensions:
50 x 2.1mm
Particle size:
1.9µm
Pore size:
140Å
Conditions:
Mobile phase:
water:acetonitrile (45:55)
Flow:
0.4mL/min.
Temp.:
25°C (or ambient)
Det.:
UV@ 254nm
Peak List:
1. uracil
3.00mg/mL
2. benzene
0.02mg/mL
3. naphthalene
0.50mg/mL
4. biphenyl
0.06mg/mL
Performance:
(calculations for biphenyl)
Efficiency:
217,619 n/m
Asymmetry:
1.10
Pressure:
4,500 psi
LC_EX0427
Figure2
—Excellent peak symmetryandefficiencyona1.9μmPinnacle™DBC18
column, usinga reversedphase testmix.
also
available
Pinnacle™DBC18Columnsalsoareavailable in
3μmand5μmparticlesizes.
Pinnacle™DBC18Columns (USPL1)
2.1mm ID
Length
cat.#
price
3µmColumns
30mm
9414332
$309
50mm
9414352
$324
100mm
9414312
$346
5µmColumns
30mm
9414532
$268
50mm
9414552
$303
100mm
9414512
$324
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