Chromatography Columns 2013+ - page 348

RefinerygasonanRt®-AluminaBOND /Na
2
SO
4
800-356-1688or 814-353-1300
4
Traces of water in the carrier
gas and sampleswill affect
the retention and selectivity of
alumina. If exposed towater,
the retention timeswill short-
en.The column can be regen-
erated by conditioning for 15-
30min. at 200°C under normal
carrier gas flow. Periodic con-
ditioning ensures excellent
run-to-run retention time
reproducibility.
Themaximum programmable
temperature for an
Rt
®
-AluminaBOND column is
200°C. Higher temperatures
cause irreversible changes to
the porous layer adsorption
properties.
ID
df (µm)
temp. limits
30-Meter
50-Meter
0.32mm 5
to 200°C
19757
19758
0.53mm 10
to 200°C
19755
19756
ID
df (µm)
temp. limits
30-Meter
50-Meter
0.32mm 5
to 200°C
19761
19762
0.53mm 10
to 200°C
19759
19760
tech
tip
NEW!
Rt
®
-AluminaBOND columns now
availablewithKCl deactivation!
Rt®-AluminaBONDColumns
• Applications forC1-C10 volatile hydrocarbon separations at percent levels, aswell as impurity
analyses at ppm concentrations.
• High capacity and loadability give exceptionally symmetric peaks.
• Reproducible retention times andpredictable flowbehavior column-to-column.
Rt®-AluminaBOND /Na
2
SO
4
• Acetylene/propadiene elute after butanes (impurities in acetylene/propadiene).
• Best separation for butene isomers (impurities inbutene streams).
• Methyl acetylene elutes after 1,3-butadiene.
• Cyclopropane (impurity inpropylene) eluteswell before propylene.
Rt®-AluminaBOND /KCl
• Acetylene elutes beforeC4hydrocarbons (impurities inbutane/isobutane).
• Methyl acetylene (impurity in1,3-butadiene) elutes before 1,3-butadiene.
1. methane
2. ethane
3. ethylene
4. propane
5. propylene
6. isobutane
7.
n
-butane
8. propadiene
9. acetylene
10.
trans
-2-butene
11. 1-butene
12. isobutylene
13.
cis
-2-butene
14. isopentane
15.
n
-pentane
16. 1,3-butadiene
17.
trans
-2-pentene
18. 2-methyl-2-butene
19. 1-pentene
20.
cis
-2-pentene
21. hexanes
Column:
Rt
®
-Alumina BOND /Na
2
SO
4
, 50m, 0.53mm ID, 10µm (cat.# 19756)
Sample:
refinery gas
Inj.:
10µL split (split vent flow 80mL/min.), 2mm single gooseneck liner (cat.# 20795)
Inj. temp.:
200°C
Carrier gas:
hydrogen, constant pressure, 8.0psi
Linear velocity: 74cm/sec.@ 45°C
Oven temp.:
45°C (hold 1min.) to 200°C@ 10°C/min. (hold 3.5min.)
Det.:
FID@ 200°C
GC_PC01085
1...,338,339,340,341,342,343,344,345,346,347 349,350,351,352,353,354,355,356,357,358,...
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