692
GCCHROMATOGRAMS |
PHARMACEUTICAL
Antiepileptics
Antiepileptics (Underivatized)
Rtx®-20
Column:
Rtx
®
-20, 15m, 0.32mm ID, 0.50µm
(cat.# 10336)
Sample:
1.0µL split injection of antiepileptic drugs
Conc.:
1,000ng/µL
Oven temp.:
150°C to 280°C@
7°C/min. (hold 5min.)
Inj./det. temp.:
250°C/270°C
Det.:
FID
Carrier gas:
helium
Linear velocity:
30cm/sec. set@ 150°C
FID sensitivity:
1.28 x 10
-10
AFS
Split ratio:
30:1
1
min.
5
10
15
20
2
3 4
5
6
7
8 9
10
11
12
GC_PH00265
Antiepileptics (Underivatized)
Rtx®-1701
1. valproic acid
2. ethosuximide
3. methsuximide
4. phensuximide
5. desmethyl methsuximide
6. mephenytoin
7. ethotoin
8. PEMA
9. phenobarbital
10. primidone
11. carbamazepine
12. diphenylhydantoin
Column:
Rtx
®
-1701, 15m, 0.32mm ID, 0.50µm
(cat.# 12036)
Sample:
1.0µL split injection of antiepileptic drugs
Conc.:
1,000ng/µL
Oven temp.:
150°C to 280°C@
7°C/min. (hold 5min.)
Inj./det. temp.:
250°C/270°C
Det.:
FID
Carrier gas:
helium
Linear velocity:
30cm/sec. set@ 150°C
FID sensitivity:
1.28 x 10
-10
AFS
Split ratio:
30:1
GC_PH00266
1
min.
5
10
15
20
2
3
4
5
6
7
8
9
10
11
12
Website :
E-mail :
TelNo : 03 9762 2034 . . . inAUSTRALIA
Mar 2011
