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125

GC COLUMNS |

PLOT COLUMNS

Fused Silica Molecular Sieve 5A Columns

similar

phases

HP PLOT Molesieve, CP-Molsieve 5A,

Molsieve 5A, AT-Molsieve, PLT-5A

tech tip

Molecular sieve materials

are very hydrophilic

Because molecular sieve materials are

very hydrophilic, they will adsorb water

from the sample or carrier gas. Water

contamination can have a detrimental

effect on peak symmetry and can reduce

the resolution of all compounds. If

water contamination occurs, reactivate

your Rt®-Msieve 5A PLOT column by

conditioning at 300 °C with dry carrier

gas flow for 3 hours.

did you know?

Rt®-Msieve 5A PLOT columns are designed

for efficient separation of Ar/O

2

and other

permanent gases, including CO.

also

available

Metal MXT®

PLOT Columns

See

page 129

.

Separation of Argon/Oxygen and Other Permanent Gases on

Rt®-Msieve 5A

GC_PC00898

Column

Rt®-Msieve 5A, 30 m, 0.53 mm ID, 50 µm (cat.# 19723)

Sample

Permanent gases

Injection

Sample valve

Sample Loop Vol.: 5 µL

Valve Name:

6-port Valco® valve

Inj. Temp.:

200 °C

Valve Temp.:

Ambient

Oven

Oven Temp.:

27 °C (hold 5 min) to 100 °C at 10 °C/min (hold 5 min)

Carrier Gas

He, constant flow

Flow Rate:

5.0 mL/min

Detector

Valco® helium ionization detector @ 150 °C

Peaks

Conc.

(µg/mL)

1. Hydrogen

40

2. Argon

30

3. Oxygen

50

4. Nitrogen

50

5. Methane

40

6. Carbon monoxide

50

Argon resolved

from oxygen.

Excellent

peak shape

for carbon

monoxide.

Rt®-Msieve 5A Columns

(fused silica PLOT)

• Improve accuracy with sharp, symmetrical peaks for argon, oxygen, and carbon

monoxide.

• Easily separate permanent gases at temperatures above ambient.

• Restek® PLOT technology reduces particle release, improving flow reproducibility

and reducing downtime for maintenance.

• Stable to 300 °C.

Molecular Sieve 5A PLOT Columns

Restek’s molecular sieve 5A PLOT columns are designed for efficient separation of

argon/oxygen and other permanent gases, including carbon monoxide. Special coating

and deactivation procedures ensure chromatographic efficiency and the integrity of

the porous layer coating. Molecular sieves have very high retention, allowing separa-

tions of permanent gases at temperatures above ambient. Our deactivation technol-

ogy also allows carbon monoxide to elute as a sharp peak. Additionally, our unique

immobilization process guarantees that the uniform particles remain adhered to the

tubing—even after continuous valve-cycling.

15-Meter

30-Meter

ID

df

temp. limits

cat.#

price

cat.#

price

0.25 mm 20 µm to 300 °C

19773

0.32 mm 30 µm to 300 °C

19720

19722

0.53 mm 50 µm to 300 °C

19721

19723