USP Solvents
Experimental Fluorinated Polymer “Tail”
1. formaldehyde
2. water
3. chloromethane
4. methanol
5. acetaldehyde
6. ethylene oxide
7. chloroethane
8. ethanol
9. acetonitrile
10. acetone
11. 2-propanol
12. 2-chloropropane
13. diethylether
14. pentane
15. ethyl formate
16. formic acid
17. methylal
18. 1,1-dichloroethene
19. methyl acetate
20. methylene chloride
21. nitromethane
22. 1-propanol
23.
trans
-1,2-dichloroethene
24. methyl
tert
-butyl ether
25. 2-methylpentane (spiked at 9%)
26. 2-butanone (MEK)
27. 2-butanol
28.
cis
-1,2-dichloroethene
29. acetic acid
30. isopropyl ether
31. ethyl acetate
32. hexane
33. chloroform
34. tetrahydrofuran
35. 2-methoxyethanol
36. 1,2-dichloroethane
37. methyl cyclopentane
38. 1,1,1-trichloroethane
39. 1,2-dimethoxyethane
40. methyl isopropyl ketone
41. 2,2-dimethoxypropane
42. isopropyl acetate
43. 1-butanol
44. benzene
45. carbon tetrachloride
46. ethylene glycol
47. formamide
48. 1,4-dioxane
49. trichloroethene
50. isooctane
51. 2-ethoxyethanol
52.
n
-heptane (C7)
53. isoamyl alcohol
54. hexanone (MIBK)
55. pyridine
56. methyl cyclohexane
57. dimethyl formamide (DMF)
58. 1,1,2-trichloroethane
59. 1-pentanol
60. isobutyl acetate
61. toluene
62. 2-hexanone (MBK)
63. dimethyl sulfoxide
64. butyl acetate
65. 1,1-diethoxypropane
66. N,N-dimethylacetamide
67. chlorobenzene
68. ethylbenzene
69. isoamyl acetate
70.
p
-xylene
71.
m
-xylene
72.
o
-xylene
73. anisole
74. isopropylbenzene (cumene)
75. 1-methyl-2-pyrrolidinone
76. sulfolane
77. 1,2,3,4-tetrahydronaphthalene
*paraldehyde
Experimental Fluorinated Polymer “Tail” 60m, 0.53mm, 3.00µm
Sample:
solvents
Conc.:
solventlessmixture ~1.3% each*
Sample size:
needle vapor
Inj.:
split, 250°C
Septa purge:
5mL/min.
Split vent flow: 100mL/min. ~1:13 split
Carrier:
helium
Head pressure: 11.0psi constant pressure
Linear velocity: 45.6 cm/sec@ 35°C
Det:
Mass Selective
Scan range:
10amu to 260amu
MS interface: open split interface ~1:7 split
Oven temp.:
35°C (hold 4min.) to 250°C@ 4°/min.
GC_EV00589
