SRITN12 - page 235

\ Figure 21 Figure 22
TRACEACETAlDEHYDE TEQUILAHEADSPACE , .
INAIR2500 ppm Column: 3' x 118" 55 packed
Column: 3' )( 118" SS wilhHayeSepti 0
packed with 801120mesh
Haye~ 0 ColumnTemp: 1000
loot120 mesh Injector Temp : 140"C
Column Temp: ,OOC'C Detector. P.E. 900 tc,
InjectOrTemp: 1..aec 22S rna 140"C
Detecl:or. P.E. 900 tc, Flow: He 30 cc/min
225 rna 14O"C sample: VaJco valve
Fiow: He30cclmin 100 microliters
Sample: Vslcovalve
100micfOlitefS
•
•
•
1. lIS M. l' 1
2. CarbOn Diolcide AlU<,
1. Air 'WO<M A1t.xl
~- ........... ....." .- --- An.xl LL
2500 ppm (wi. ) .."""'" ....., 8
- . .,-
• • • ........ ........
,
........
TRACE AU:OHOLS
"WATER
Column: 10' x 118" packed
with Hayesep- 0
8lli1OO mesh
ColumnTemp: 7S-c up to
150"0 at 1S-elmin
Flow: He 33 ccImin
IriedDr TenIp;125'C
D«edor: PoE.900 rc ,..ma
An. x 114Q-C
Sample: 3 microliters
1._""ppm
~..-"'ppm
\
"'J
, , .
• • _.
Agure24
HYDROGENSULPHIDE
Column: 10' )( W" Ni packed
withHaye&pe 0
10Q(120 mesh
ColumnTemp: 6O"C
InjectorTemp: l00"C
Detector:P.E. 900T,C.
225 rna l4O"C
Flow: He30celmin
sample: YaJoo vaNe
50 microliters vapor
(ambient)
1. Ait~}
2. CartIon 0itIQde appYJlt 0.1%
3. ........ approK 2,5Ill,
.. H)OoOIn SuIphidI apptOlt 2.5%
•
.
• •
- ,..