SRITN12 - page 145

Theory of Operation continued
POPULAR CONFIGURATION GCs
BTEX & Environmental
RoomTemperatureManual Headspace Injection
WhenmakingheadspaceinjectionswiththeBTEXorEnvironmentalGCsystems,thesampleisequilibrated
offlineat room temperature. It is then injectedbysyringe into theon-column injector. This technique is
basically thedirect injectionofsmallgassamples.
GasSampleConcentration
In thisTO-14 type technique, a largevolumeofgas ispushedbysyringeorpulledbyvacuumpump
through thedual traps. The trappedanalytesare thendesorbedandswept into thecolumn. If theGChas the
optionalvacuumpump interface, thepump isplugged into itandmaybecontrolledby thePeakSimpledata
systemusinganevent table.
Direct Injection
DirectinjectionwiththeBTEXorEnvironmentalGCsystemsissimpleandstraightforward. Thismethod
uses theon-column injector to inject thesampledirectly into thecolumn,bypassing theentirepurgeand trap
injectionsystem. Samplesizefor this technique is1mLor lessforgas,and5µLor lessfor liquid. Noevent
table isnecessary, justa temperatureprogramfor thecolumnoven.
VOAvialand1mLsyringewith27gauge
needle formanualheadspace injections
1...,135,136,137,138,139,140,141,142,143,144 146,147,148,149,150,151,152,153,154,155,...505
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