Triazines
--------------0
~TM
5-MS ;
ultra-Iovv bleeding column
Conditions
*
OvenProgram: 60°C(5min), 8°0min, 300°C(IOmin).
CarrierGas: Helium, l.5mUmin,constant flow.
Injector:Split275°C,30mUminsplitflow (IminSplitless).
MS: transferline300°C,source 225°C,segmented scan 45-450amu.
Column:
MEGA-5 MSXii - O.25mm,O.25IJm, 30m
CatalogCode:MS-5XIL-025-025-30
Absolute standard mix
#
40017 (I
ngl~L
each compound).
EPAmethod 619
2
Acknowledgement:
Cromlab
S.L.,Acer 30-32.08038Barcelona.
3
4
5 7
6
8
9
IS
IS
10
12
II
13
14
mega
I.Atrazine-desisopropyl
2.
Atrazine-desethyl
3.
Terbuthylazine
4.Atraton
5.Simazine
6.
Prometon
7.
Atrazine
8.
Propazine
9.Terbuthylazine
10.Secbumeton
I I.
Simetryne
I2.
Ametryn
13.Prometryne
14.Terbutryn
26
min
TICMS
iJ: conditions usedarenotoptimized forseparations butarestandard conditions usedfora round-robin comparison.
HROIIII""" .J'#"I«::
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