TCDDs Isomers
------------------0
~TM
5-MS ;
ultra-Iovv bleeding column
100
.
'"
Conditions
OvenProgram: 160°C, 10oOmin, 190°C, 2.so0min,255°C,
4°0min, 310°C.
CarrierGas: Heliumpressure programmed from
400kPa
to
526kPa
@
3kPa/min.
Injector:directdeactivated glass liner, heated
@
260°C.
16.69
16.69 - 13C12-I,2,3,4 -TCDD
17.27 - 13C12-2,3,7,8 -TCDD
17.27
1:Voltage SIR17ChannelsEI+
333.9339
1.5687
Column:
MEGA-5
MSf)(jj7~m,
0.1OlJm, 30m
CatalogCode:MS-5XIL-015-0I0-30
RetentionGap:
DPTMDS0.25mm, 2.5m
CatalogCode:RETG-DPTMDS-025-2-5
Connector:
Press-Fit Union
CatalogCode:PFITUN-O15-025-1
meets and far exceeds the
EPAmethod 8280 resolution criteria
8
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