POCs
--------------0
~TM
5-MS ;
ultra-Iovv bleeding column
OvenProgram: 60°C(5min),8°0min, 300°C(IOmin).
CarrierGas: Helium, l.5mUmin,constantflow.
Injector:Split275°C,30mUminsplitflow (IminSplitless).
MS: transferline300°C,sounce 225°C,segmented scan 45-450amu.
Conditions
*
meae
Column: MEGA-S MSXii - <t.'1Smm,O.2SlJm, 30m
CatalogCode:MS-5XIL-025-025-30
20,21
19
13.Heptachlor
14.DCPA
15.Aldrin
16.lsodrin
17.Heptachlor-epoxide
18.Captan
19.gamma-Chlordane
20.alpha-Chlordane
21.Endosulfan-I
22.t-Nonachlor
23.pp-DDE
24.Dieldrin
25.Endrin
26.Perthane
27.Chlorobenzilate
28.Endosulfan-II
29.c1s-Nonachlor
30.pp-DDD
31.Endrinaldehyde
32.Carbophenothion
33.Endosulfan sulfate
34.pp-DDT
35.Endrinketone
36.Methoxychlor
37.Mirex
38.c-Permethrin
39.t-Permethrin
AccustandardmixM-680p,MS08P-B-Rand M-617-2(I
ngl~L
each compound).
I.Etridiaziole
2.Chioroneb
3.Propachlor
4.Trifluralin
5.alpha-HCH
6.HCB
7.Dicloran
8.Quintozene
9.beta-HCH
10.gamma-HCH
I I.Chlorotalonil
12. delta-HCH
36
EPAmethod617
9 10
EPAmethod508
IS
2
4
5
6
3
8
IS
II
IS /
12
13
14
15
16 17
23 25,26
29
27
30
.>
28
34
22
/
24
33
35
31 32
37
7
18
38
39
32.Smin
Acknowledgement: CromlabS.L.,Acer30-32,08038Bancelona.
TIC MS
It:
conditionsusedarenot optimizedfor separations but arestandard conditionsusedfor around-robincomparison.
HROIIII""" .J'#"I«::
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