665
GCCHROMATOGRAMS |
CLINICAL, FORENSIC&TOXICOLOGY
Arson Accelerants
UnleadedGasoline
Rxi®-1ms
Column:
Rxi
®
-1ms, 30m, 0.25mm ID, 0.25µm (cat.# 13323)
Sample:
5,000µg/mL unleaded gasoline, unweathered, inmethanol
(cat.# 30096)
Inj.:
1µL split (split ratio 20:1), 4mm single gooseneck liner w/wool
(cat.# 22405)
Inj. temp.:
250°C
Carrier gas:
helium, constant flow
Linear velocity: 28cm/sec.@ 50°C
Oven temp.:
50°C (hold 2min.) to 75°C@ 10°C/min. to 300°C@ 20°C/min.
(hold 5min.)
Det.:
FID@ 300°C
GC_PC01071
99%WeatheredUnleadedGasoline
Rxi®-1ms
Column:
Rxi
®
-1ms, 30m, 0.25mm ID, 0.25µm (cat.# 13323)
Sample:
5,000µg/mL unleaded gasoline, 99%weathered, inmethanol
(cat.# 30436)
Inj.:
1µL split (split ratio 20:1), 4mm single gooseneck liner w/wool
(cat.# 22405)
Inj. temp.:
250°C
Carrier gas:
helium, constant flow
Linear velocity: 28cm/sec.@ 50°C
Oven temp.:
50°C (hold 2min.) to 75°C@ 10°C/min. to 300°C@ 20°C/min.
(hold 5min.)
Det.:
FID@ 300°
GC_PC01070
UnweatheredKerosene
Rxi®-1ms
GC_PC01060
Column:
Rxi
®
-1ms, 30m, 0.25mm ID, 0.25µm (cat.# 13323)
Sample:
5,000µg/mL kerosene, unweathered, inmethylene chloride (cat.# 31229)
Inj.:
1µL split (split ratio 20:1), 4mm single gooseneck liner w/wool (cat.# 22405)
Inj. temp.:
250°C
Carrier gas:
helium, constant flow
Linear velocity: 28cm/sec.@ 50°C
Oven temp.:
50°C (hold 2min.) to 75°C@ 10°C/min. to 300°C@ 20°C/min. (hold 5min.)
Det.:
FID@ 300°C
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Mar 2011
