001_TOC.qxp - page 119

660
GCCHROMATOGRAMS |
PETROLEUM&PETROCHEMICAL
Hydrocarbons (Simulated Distillation)
SimulatedDistillation
(StandardCalibration)
MXT®-1SimDist
3
2
5
4
6
7
8
9
10
11 12
13 14
15
16
17
min.
4
8
12
16
20
24
1. C6
2. C7
3. C8
4. C9
5. C10
6. C11
7. C12
8. C14
9. C16
10. C18
11. C20
12. C24
13. C28
14. C32
15. C36
16. C40
17. C44
1
GC_PC00224
Column:
MXT
®
-1 SimDist, 6m, 0.53mm ID, 0.15µm (cat.# 70101)
Sample:
wet needle on-column injection of ASTMD2887 standard
Oven temp.:
-12°C to 430°C@ 20°C/min.
Inj./det. temp.: -17°C to 433°C/430°C
Carrier gas:
hydrogen
Linear velocity:
40cm/sec.
FID sensitivity:
128 x 10
-11
AFS
SimulatedDistillation
(High-Temperature)
MXT®-500SimDist
Column:
MXT
®
-500 SimDist, 6m, 0.53mm ID, 0.15µm (cat.# 70104)
Sample:
cold on-column injection of Polywax
®
655 in CS
2
Oven temp.:
40°C to 430°C@ 6°C/min.
Carrier gas:
helium
Linear velocity:
40cm/sec.
FID sensitivity:
2 x 10
-11
AFS
20 24 28 32 36 40 44 48 52 56 60 64 68
min.
GC_PC00225
GC_PC00750
SimulatedDistillation
Rtx®-2887
Column:
Rtx
®
-2887, 10m, 0.53mm ID, 2.65µm (cat.# 10199)
Sample:
1µL direct injection of 0.01-0.1wt. % C5 to C44 hydrocarbon standard
in carbon disulfide
Inj. temp.:
360°C
Det. temp:
360°C
Carrier gas:
helium (constant flow)
Linear velocity: 15mL/min. (112cm/sec.)
Oven temp.:
35°C to 360°C@ 15°C/min. (hold 5min.)
1. C5
2. C6
3. C7
4. C8
5. C9
6. C10
7. C11
8. C12
9. C14
10. C16
11. C18
12. C20
13. C24
14. C28
15. C32
16. C36
17. C40
18. C44
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TelNo : 03 9762 2034 . . . inAUSTRALIA
Mar 2011
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