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179

PAH Mix on Pinnacle® DB PAH

LC COLUMNS

Application-Specific Columns

Restek-

manufactured

silica

Chromatographic Properties

Specifically designed to resolve complex mixtures of polycyclic aromatic hydrocarbons (PAHs).

Get complete resolution of all 16 EPA 610 PAHs, plus two other routinely analyzed PAH com-

pounds, in less than five minutes to greatly reduce run times and increase sample throughput.

Column Characteristics:

particle size:

1.9 µm, spherical

pore size:

140 Å

end-cap:

no

pH range:

2.5 to 8

temperature limit: 80 °C

Pinnacle® DB PAH UHPLC Columns

2.1 mm ID

Length

cat.#

price

1.9 µm Columns

30 mm

9470232

50 mm

9470252

100 mm

9470212

0.00

0.50

1.00

1.50

2.00

2.50

3.00

3.50

4.00

4.50

5.00

Time (min)

1

2 3 4 5

6

7

8

9 10

11

12

13

14

15

16

17

18

LC_EV0521

Column

Pinnacle® DB PAH (cat.# 9470252)

Dimensions:

50 mm x 2.1 mm ID

Particle Size:

1.9 µm

Pore Size:

140 Å

Temp.:

30 °C

Sample

EPA Method 8310 PAH Mixture (cat.# 31841)

Diluent:

acetonitrile

Conc.:

10 µg/mL

Inj. Vol.:

1 µL

Mobile Phase

A:

water

B:

acetonitrile

Time (min) Flow (mL/min) %A

%B

0

0.8

60

40

2

0.8

40

60

4

0.8

0

100

4.5

0.8

0

100

4.51

0.8

60

40

5

0.8

60

40

Max Pressure:

724 bar

Detector

Photo diode array @ 254, 4.8 nm

Instrument

Waters

Peaks

1. Naphthalene

2. Acenaphthylene

3. 1-Methylnaphthalene

4. 2-Methylnaphthalene

5. Acenaphthene

6. Fluorene

7. Phenanthrene

8. Anthracene

9. Fluoranthene

10. Pyrene

11. Benzo[a]anthracene

12. Chrysene

13. Benzo[b]fluoranthene

14. Benzo[k]fluoranthene

15. Benzo[a]pyrene

16. Dibenzo[a,h]anthracene

17. Benzo[ghi]perylene

18. Indeno[1,2,3-cd]pyrene