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ANALYTICALREFERENCEMATERIALS |
ENVIRONMENTALMATERIALS
Minnesota Dept. of Agriculture Pesticides
MinnesotaDept.ofAgricultureList1PesticidesonanRxi®-1mscolumn.
acetochlor
alachlor
atrazine
cyanazine
desethylatrazine
desisopropylatrazine
dimethenamid*
ethalfluralin
metolachlor
metribuzin
pendimethalin
prometon
propachlor
propazine
simazine
trifluralin
*Added toMinnesotaDepartment of Agriculture List 1 pesticide (neutrals) inci-
dent investigation requirements, effective January 1, 2000.¹ CAS# 87674-68-8
manufactured by several companies under various trade names.
¹Analytical Lists for Pesticide Incident Investigations, MinnesotaDepartment of
Agriculture, GuidanceDocument 26 (3/99), St. Paul, MN. For a copy, visit their
web site at:
MinnesotaAgList1PesticidesMixA
(16 components)
200ppm each in acetone, 1mL/ampul
cat.# 32406 (ea.)
chlorpyrifos
EPTC
fonofos
phorate
terbufos
triallate
MinnesotaAgList1PesticidesMixB
(6 components)
200ppm each in acetone, 1mL/ampul
cat.# 32407 (ea.)
MinnesotaDepartmentofAgricultureList 1Pesticides
GC_EV00837
1. 2-fluorophenol (SS)
2. phenol-d6 (SS)
3. 1,4-dichlorobenzene-d4 (IS)
4. nitrobenzene-d5 (SS)
5. naphthalene-d8 (IS)
6. EPTC
7. 2-fluorobiphenyl (SS)
8. acenaphthene-d10 (IS)
9. propachlor
10. desisopropyl atrazine
11. desethyl atrazine
12. 2,4,6-tribromophenol (SS)
13. ethalfluralin
14. trifluralin
15. phorate
16. simazine
17. prometon
18. atrazine
19. propazine
20. terbufos
21. fonofos
22. phenanthrene-d10 (IS)
23. triallate
24. metribuzin
25. dimethenamid
26. acetochlor
27. alachlor
28. cyanazine
29. metolachlor
30. chlorpyrifos
31. pendimethalin
32.
p
-terphenyl-d14 (SS)
33. chrysene-d12 (IS)
34. perylene-d12 (IS)
Column:
Rxi
®
-1ms, 30m, 0.25mm ID, 0.25µm
(cat.# 13323)
Sample:
Minnesota Ag List 1 PesticidesMix A
(cat.# 32406),
Minnesota Ag List 1 PesticidesMix B
(cat.# 32407),
SV Internal StandardMix (cat.# 31206),
B/N SurrogateMix (4/89 SOW)
(cat.# 31024),
Acid SurrogateMix (4/89 SOW)
(cat.# 31025)
Inj.:
1.0µL, 10µg/mL each analyte
(internal standards 25µg/mL), split (10:1)
4mmDrilledUniliner
®
inlet liner
(hole near bottom) (cat.# 20771)
Instrument:
Agilent 6890
Inj. temp.:
250°C
Carrier gas:
helium, constant flow
Flow rate:
1.2mL/min.
Oven temp.:
70°C (hold 1min.) to 180°C@ 20°C/min.,
to 230°C@ 5°C/min., to 325°C@
40°C/min. (hold 3.5min.)
Det.:
Agilent 5973MSD
Transfer line
temp.:
280°C
Scan range:
35-550amu
Solvent delay:
2.50min.
Tune:
DFTPP
Ionization:
EI
Contains 1mL each of thesemixtures.
32406: Minnesota Ag List PesticidesMix A
32407: Minnesota Ag List PesticidesMix B
Quantity discounts not available.
MinnesotaAgList1PesticideKit
cat.# 32408 (kit)
kit
also
available
See
page41
forour Rxi®-1ms capillarycolumns.
Website :
E-mail :
TelNo : 03 9762 2034 . . . inAUSTRALIA
Mar 2011
