485
REFERENCESTANDARDS |
ENVIRONMENTALMATERIALS
8000 Series Methods
Ultra II®Aromaxcolumnsseparateall17 targetcompoundsandcanbeusedalone (MS)orwitha
confirmationcolumn (UV).
Method8330 (NitroaromaticsandNitraminesbyHPLC)
cont'd
also
available
Seematerials forGCMethod8095on
pages473-474.
also
available
Ultra II®AromaxHPLC
columns,
page161
UltraC18HPLCcolumns,
page182
Compound
Solvent
Conc.
cat.# (ea.)
price
2-amino-4,6-dinitrotoluene
ACN 1,000
31670
4-amino-2,6-dinitrotoluene
ACN 1,000
31671
ammonium picrate*
ACN 2,000
31890
3,5-dinitroaniline
ACN 1,000
31661
1,2-dinitrobenzene
M 1,000
31453
1,3-dinitrobenzene
ACN 1,000
31662
2,4-dinitrotoluene
ACN 1,000
31663
2,6-dinitrotoluene
ACN 1,000
31664
3,4-dinitrotoluene
EA 2,000
33901
3,4-dinitrotoluene
M 1,000
31452
EGDN*
M 1,000
31601
HMX*
ACN 1,000
31665
2-methyl-4-nitroaniline
M 1,000
31612
nitrobenzene
ACN 1,000
31657
nitroglycerin*
M 1,000
31498
nitroguanidine*
M 1,000
31602
2-nitrotoluene
ACN 1,000
31659
3-nitrotoluene
ACN 1,000
31660
4-nitrotoluene
ACN 1,000
31658
PETN (pentaerythritol tetranitrate)* M 1,000
31600
picric acid*
M 1,000
31499
propylene glycol dinitrate (PGDN)
M 1,000
31821
RDX*
ACN 1,000
31666
tetryl*
ACN 1,000
31667
1,3,5-trinitrobenzene*
ACN 1,000
31668
2,4,6-trinitrotoluene*
ACN 1,000
31669
ACN= acetonitrile; EA= ethyl acetate; M=methanol
Single-ComponentExplosivesSolutions
Volume is 1mL/ampul. Concentration is µg/mL.
*Meet all DOT requirements. Available only to customers or distributors inside
the 48 contiguous United States; itemsmay not be resold for export.
Contains 1mL each of thesemixtures.
31450: 8330 CalibrationMix#1
31451: 8330 CalibrationMix#2
31452: 8330 Internal StandardMix
31453: 8330 SurrogateMix
Quantity discounts not available.
8330NitroaromaticsKit (1,000μg/mL)
cat.# 31454 (kit)
kit
1. HMX
2. RDX
3. nitroglycerin
4. nitrobenzene
5. 4-amino-2,6-dinitrotoluene
6. 3,5-dinitroaniline
7. 2-nitrotoluene
8. 2-amino-4,6-dinitrotoluene
9. 3-nitrotoluene
10. PETN
11. 4-nitrotoluene
12. 1,3-dinitrobenzene
13. 2,6-dinitrotoluene
14. tetryl
15. 2,4-dinitrotoluene
16. 1,3,5-trinitrobenzene
17. 2,4,6-trinitrotoluene
Sample:
8330BNitroaromatics andNitramineMix
(cat.# 33204)
Inj.:
10µL
Conc.:
10µg/mL each component
Sample diluent: methanol
Column:
Ultra II
®
Aromax
Cat.#:
9607575
Dimensions:
250mm x 4.6mm
Particle size:
5µm
Pore size:
100Å
Conditions:
Instrument:
Shimadzu ProminenceUFLCXR
Mobile phase:
water:methanol, 35:65 (v/v)
Flow:
1.2mL/min.
Temp.:
30°C
Det.:
UV@ 254nm and 210nm
LC_EV0484
free
literature
Formore information, downloadour
Analysisof
ExplosivesbyLiquidChromatography
applications
note from
lit. cat.#EVAN1176
Website :
E-mail :
TelNo : 03 9762 2034 . . . inAUSTRALIA
Mar 2011
