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Conditions for BothColumns: Inj: 1.0uL splitless (0.5minhold), 4mmDrilledUniliner inlet sleeve
Inj. Temp: 225°C Carrier gas: hydrogen, constant pressure, 71cm/sec@140°C
Oven temp: 140°C(0.5min) to268°C@ 30°C/min (0min), to290°C@11°C/min (0min), to330°C@25°C/min (5min)
Figure1a: Rtx-440 30m x 0.32mm, 0.50µm
cat#12939
1. TCX
2.
α
-BHC
3.
γ
-BHC
4.
β
-BHC
5.
δ
-BHC
6. heptachlor
7. aldrin
8. heptachlor epoxide
9.
γ
-chlordane
10.
α
-chlordane
11. endosulfan 1
12. 4,4’-DDE
13. dieldrin
14. endrin
15. 4,4'-DDD
16. endolsulfan II
17. endrin aldehyde
18. 4,4'-DDT
19. endosulfan sulfate
20.methoxychlor
21. endrinketone
22. decachlorobiphenyl
