Restek 2011/12 Chromatography Catalog - page 660

660
GC CHROMATOGRAMS |
PETROLEUM & PETROCHEMICAL
Hydrocarbons (Simulated Distillation)
Simulated Distillation
(Standard Calibration)
MXT®-1 Sim Dist
3
2
5
4
6
7
8
9
10
11 12
13 14
15
16
17
min.
4
8
12
16
20
24
1. C6
2. C7
3. C8
4. C9
5. C10
6. C11
7. C12
8. C14
9. C16
10. C18
11. C20
12. C24
13. C28
14. C32
15. C36
16. C40
17. C44
1
GC_PC00224
Column:
MXT
®
-1 Sim Dist, 6m, 0.53mm ID, 0.15µm (cat.# 70101)
Sample:
wet needle on-column injection of ASTM D2887 standard
Oven temp.:
-12°C to 430°C @ 20°C/min.
Inj./det. temp.: -17°C to 433°C/430°C
Carrier gas:
hydrogen
Linear velocity:
40cm/sec.
FID sensitivity:
128 x 10
-11
AFS
Simulated Distillation
(High-Temperature)
MXT®-500 Sim Dist
Column:
MXT
®
-500 Sim Dist, 6m, 0.53mm ID, 0.15µm (cat.# 70104)
Sample:
cold on-column injection of Polywax
®
655 in CS
2
Oven temp.:
40°C to 430°C @ 6°C/min.
Carrier gas:
helium
Linear velocity:
40cm/sec.
FID sensitivity:
2 x 10
-11
AFS
20 24 28 32 36 40 44 48 52 56 60 64 68
min.
GC_PC00225
GC_PC00750
Simulated Distillation
Rtx®-2887
Column:
Rtx
®
-2887, 10m, 0.53mm ID, 2.65µm (cat.# 10199)
Sample:
1µL direct injection of 0.01-0.1 wt. % C5 to C44 hydrocarbon standard
in carbon disulfide
Inj. temp.:
360°C
Det. temp:
360°C
Carrier gas:
helium (constant flow)
Linear velocity: 15mL/min. (112cm/sec.)
Oven temp.:
35°C to 360°C @ 15°C/min. (hold 5 min.)
1. C5
2. C6
3. C7
4. C8
5. C9
6. C10
7. C11
8. C12
9. C14
10. C16
11. C18
12. C20
13. C24
14. C28
15. C32
16. C36
17. C40
18. C44
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Mar 2011
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