635
GC CHROMATOGRAMS |
FOODS, FLAVORS & FRAGRANCES
Food Contaminants
Organochlorine and Organophosphorus Pesticides
FAPAS® Proficiency Testing
Rxi®-5ms
GC_FF00826
1. dichlorvos
2. methacrifos
3.
α
-BHC
4. hexachlorobenzene
5.
δ
-BHC (lindane)
6.
β
-BHC
7. diazinon
8. etrimphos
9. phosphamidon
10. chlorpyrifos-methyl
11. heptachlor
12. fenitrothion
13. pirimiphos methyl
14. malathion
15. aldrin
16. chlorpyrifos
17. heptachlor epoxide
18. oxychlordane
19.
trans
-chlordane
20. endosulfan I
21.
cis
-chlordane
22. 2,4'-DDT
23. dieldrin
24. endrin
25. endosulfan II
26. 4,4'-DDE
27. 4,4'-DDD
28. endosulfan sulfate
29. 4,4'-DDT
Column:
Rxi
®
-5ms, 30m, 0.25mm ID, 0.25µm
(cat.# 13423)
Sample:
FAPAS Series 5 OC Pesticide Mix 1
(cat.# 32412),
FAPAS Series 9 OP Pesticide Mix 1
(cat.# 32413)
Inj.:
1.0µL, 10ppm each analyte, split (10:1)
4mm Drilled Uniliner
®
inlet liner (hole near
bottom) (cat.# 20771)
Instrument:
Agilent 6890
Inj. temp.:
290°C
Carrier gas:
helium, constant flow
Flow rate:
1.2mL/min.
Oven temp.:
100°C (hold 0.5 min.) to 300°C @ 7°C/min.
(hold 1 min.)
Det.:
Agilent 5973 GC/MS
Transfer line
temp.:
280°C
Scan range:
35-550amu
Solvent delay:
4 min.
Tune:
DFTPP
Ionization:
EI
Organochlorine and Organophosphorus Pesticides
FAPAS® Proficiency Testing
Rxi®-5ms
1. naphthalene-d8
2. dichlorvos
3. acenaphthene-d10
4. methacrifos
5.
α
-BHC
6. hexachlorobenzene
7.
δ
-BHC (lindane)
8.
β
-BHC
9. phenanthrene-d10
10. diazinon
11. etrimphos
12. phosphamidon
13. chlorpyrifos-methyl
14. heptachlor
15. fenitrothion
16. pirimiphos methyl
17. malathion
18. aldrin
19. chlorpyrifos
20. heptachlor epoxide
21. oxychlordane
22.
trans
-chlordane
23. endosulfan I
24.
cis
-chlordane
25. 2,4'-DDT
26. dieldrin
27. endrin
28. endosulfan II
29. 4,4'-DDE
30. 4,4'-DDD
31. endosulfan sulfate
32. 4,4'-DDT
33. chrysene-d12
34. perylene-d12
Column:
Rxi
®
-5ms, 30m, 0.25mm ID, 0.25µm
(cat.# 13423)
Sample:
FAPAS Series 5 OC Pesticide Mix 1
(cat.# 32412),
FAPAS Series 9 OP Pesticide Mix 1
(cat.# 32413),
SV Internal Standard Mix (cat.# 31206)
Inj.:
1.0µL, 10ppm each analyte,
split (10:1)
4mm Drilled Uniliner
®
inlet liner
(hole near bottom) (cat.# 20771)
Instrument:
Agilent 6890
Inj. temp.:
290°C
Carrier gas:
helium, constant flow
Flow rate:
1.2mL/min.
Oven temp.:
100°C (hold 0.5 min.) to 300°C @ 7°C/min.
(hold 1 min.)
Det.:
Agilent 5973 GC/MS
Transfer line
temp.:
280°C
Scan range:
35-550amu
Solvent delay:
4 min.
Tune:
DFTPP
Ionization:
EI
GC_FF00827
Rxi® Technology!
Exceptionally inert,
ultra low- bleed
capillary columns.
Rxi® Technology!
Exceptionally inert,
ultra low- bleed
capillary columns.
Website :
E-mail :
TelNo : 03 9762 2034 . . . in AUSTRALIA
Mar 2011
