Restek 2011/12 Chromatography Catalog - page 569

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GC CHROMATOGRAMS | ENVIRONMENTAL
Pest icides
Organochlorine Pesticide Mix AB #2
US EPA Method 8081
Rtx®-CLPesticides and Rtx®-CLPesticides2 (0.53mm ID Column Set)
Columns: Rtx®-CLPesticides, 30m, 0.53mm ID, 0.50µm (cat.# 11140) and
Rtx®-CLPesticides2, 30m, 0.53mm ID, 0.42µm (cat.# 11340) with
5m x 0.53mm ID Rxi® deactivated guard tubing (cat.# 10054),
connected using Siltek® Treated Universal “Y” Press-Tight® connector (cat.# 20486)
Sample: Organochlorine Pesticide Mix AB #2, 8-80µg/mL each component
in hexane/toluene (cat.# 32292), Pesticide Surrogate Mix, 200µg/mL
each component in acetone (cat.# 32000)
Inj.: 1.0µL splitless (hold 0.3 min.), 4mm single gooseneck inlet liner (cat.# 20799)
Inj. temp.: 250°C
Carrier gas: helium, constant flow
Linear velocity: 45cm/sec. @ 120°C
Oven temp.: 120°C to 200°C @ 45°C/min. to 230°C @ 12.5°C/min. to
320°C (hold 2 min.) @ 20°C/min.
Det.: µ-ECD @ 330°C
1. 2,4,5,6-tetrachloro- m-xylene (SS)
2. α-BHC
3. γ-BHC
4. β-BHC
5. δ-BHC
6. heptachlor
7. aldrin
8. heptachlor epoxide (isomer B)
9. γ-chlordane
10. α-chlordane
11. endosulfan I
12. 4,4'-DDE
13. dieldrin
14. endrin
15. 4,4'-DDD
16. endosulfan II
17. 4,4'-DDT
18. endrin aldehyde
19. endosulfan sulfate
20. methoxychlor
21. endrin ketone
22. decachlorobiphenyl (SS)
GC_EV00937 GC_EV00936
Rtx®-CLPesticides2 Rtx®-CLPesticides
Organochlorine Pesticide Mix AB #2
US EPA Method 8081
Rtx®-CLPesticides and Rtx®-CLPesticides2 (0.32mm ID Column Set)
Columns: Rtx®-CLPesticides, 30m, 0.32mm ID, 0.32µm (cat.# 11141) and
Rtx®-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324) with
5m x 0.32mm ID Rxi® deactivated guard tubing (cat.# 10039),
connected using Deactivated Universal “Y” Press-Tight ® connector (cat.# 20405-261)
Sample: Organochlorine Pesticide Mix AB #2, 8-80µg/mL
each component in hexane/toluene (cat.# 32292), Pesticide Surrogate Mix,
200µg/mL each component in acetone (cat.# 32000)
Inj.: 1.0µL splitless (hold 0.3 min.), 4mm single gooseneck inlet liner (cat.# 20799)
Inj. temp.: 250°C
Carrier gas: helium, constant flow
Linear velocity: 60cm/sec. @ 120°C
Oven temp.: 120°C to 200°C @ 45°C/min. to 230°C @ 15°C/min. to 330°C (hold 2 min.)
@ 30°C/min.
Det.: µ-ECD @ 330°C
1. 2,4,5,6-tetrachloro- m-xylene (SS)
2. α-BHC
3. γ-BHC
4. β-BHC
5. δ-BHC
6. heptachlor
7. aldrin
8. heptachlor epoxide (isomer B)
9. γ-chlordane
10. α-chlordane
11. endosulfan I
12. 4,4'-DDE
13. dieldrin
14. endrin
15. 4,4'-DDD
16. endosulfan II
17. 4,4'-DDT
18. endrin aldehyde
19. endosulfan sulfate
20. methoxychlor
21. endrin ketone
22. decachlorobiphenyl (SS)
GC_EV00933 GC_EV00933A
Rtx®-CLPesticides2 Rtx®-CLPesticides
0.53mm ID column analysis
performed in less than 9 min.
0.32mm ID column analysis
performed in less than 7 min.
Website :www.chromtech.net.auE-mail :info@chromtech.net.auTelNo : 03 9762 2034 . . . in AUSTRALIA Mar 2011