• 15 •
2003
Volume 2
800-356-1688
1. 1,4-dioxane
2. pyridine
3. N-nitrosodimethylamine
4. ethyl methacrylate
5. 2-picoline
6. N-nitrosomethylethylamine
7. methyl methanesulfonate
8. 2-fluorophenol (SS)
9. N-nitrosodiethylamine
10. ethyl methanesulfonate
11. benzaldehyde
12. phenol-d6 (SS)
13. phenol
14. aniline
15. pentachloroethane
16. bis(2-chloroethyl)ether
17. 2-chlorophenol
18. 1,3-dichlorobenzene
19. 1,4-dichlorobenzene-d4 (IS)
20. 1,4-dichlorobenzene
21. benzyl alcohol
22. 1,2-dichlorobenzene
23. 2-methylphenol
24. bis(2-chloroisopropyl)ether
25. acetophenone
26. 4-methylphenol/3-methylphenol
27. N-nitroso-di-
n-
propylamine
28. nitrosopyrrolydine
29.
o-
toluidine
30. 4-nitrosomorpholine
31. hexachloroethane
32. nitrobenzene-d5 (SS)
33. nitrobenzene
34. N-nitrosopiperidine
35. isophorone
36. 2-nitrophenol
37. 2,4-dimethylphenol
38. bis(2-chloroethoxy)methane
39. 2,4-dichlorophenol
40. 1,2,4-trichlorobenzene
41.
α
,
α
-dimethylphenylamine
42. naphthalene-d8 (IS)
43. naphthalene
44. 2,6-dichlorophenol
45. 4-chloroaniline
46. hexachloropropene
47. hexachlorobutadiene
48. N-nitroso-
n-
butylamine
49. 1,4-phenylenediamine
50. caprolactam
51. 4-chloro-3-methylphenol
52. isosafrole (isomer)
53. 2-methylnaphthalene
54. 1-methylnaphthalene
55. hexachlorocyclopentadiene
56. 1,2,4,5-tetrachlorobenzene
57. isosafrole (isomer)
58. 2,4,6-trichlorophenol
59. 2,4,5-trichlorophenol
60. 2-fluorobiphenyl (SS)
61. safrole
62. biphenyl
63. 2-chloronaphthalene
64. 1-chloronaphthalene
65. diphenyl ether
66. 2-nitroaniline
67. 1,4-naphthoquinone
68. 1,4-dinitrobenzene
69. dimethylphthalate
70. 1,3-dinitrobenzene
71. 2,6-dinitrotoluene
72. acenaphthylene
73. 1,2-dinitrobenzene
74. 3-nitroaniline
75. acenaphthene-d10 (IS)
76. acenaphthene
77. 2,4-dinitrophenol
78. pentachlorobenzene
79. 4-nitrophenol
80. dibenzofuran
81. 2,4-dinitrotoluene
82. 1-naphthalamine
83. 2,3,4,6-tetrachlorophenol
84. 2,3,5,6-tetrachlorophenol
85. 2-naphthylamine
86. diethyl phthalate
87. fluorene
88. 4-chlorophenyl phenyl ether
89. 2-methyl-5-nitroaniline
90. 4-nitroaniline
91. 4,6-dinitro-2-methylphenol
92. diphenylamine
93. azobenzene
94. 2,4,6-tribromophenol (SS)
95. diallate
96. 1,3,5-trinitrobenzene
97. phenacetin
98. 4-bromophenyl phenyl ether
99. hexachlorobenzene
100. atrazine
101. 4-aminobiphenyl
102. pentachlorophenol
103. pentachloronitrobenzene
104. propyzamide
105. phenanthrene-d10 (IS)
106. phenanthrene
107. anthracene
108. carbazole
109. di-
n-
butylphthalate
110. 4-nitroquinoline-1-oxide
111.methapyriline
112. isodrin
113. fluoranthene
114. pyrene
115. Aramite (isomer)
116.
p-
terphenyl-d14 (SS)
117. Aramite (isomer)
118. dimethylaminoazobenzene
119. dichlorobenzilate
120. 3,3-dimethylbenzidine
121. butyl benzyl phthalate
122. kepone
123. bis(2-ethylhexyl)adipate
124. 2-acetylaminofluorene
125. benz(a)anthracene
126. chrysene-d12 (IS)
127. chrysene
128. bis(2-ethylhexyl)phthalate
129. di-
n-
octyl phthalate
130. benzo(b)fluoranthene
131. 7,12-dimethylbenz(a)anthracene
132. benzo(k)fluoranthene
133. benzo(a)pyrene
134. perylene-d12 (IS)
135. 3-methylcholanthrene
136. dibenz(a,j)acridine
137. indeno(1,2,3-cd)pyrene
138. dibenz(a,h)anthracene
139. benzo(ghi)perylene
GC_EV00682
Rtx
®
-5Sil MS,
30m, 0.25mm ID, 0.25µm (cat.# 12723)
Sample:
8270MegaMix™ (cat.# 31686)
Appendix IXMix #1 (cat.# 31625)
Appendix IXMix #2 (cat.# 31806)
SV Internal StandardMix (cat.# 31206)
B/NSurrogateMix (4/89 SOW) (cat.# 31062)
Acid SurrogateMix (4/89 SOW) (cat.# 31063)
50ng each analyte on-column
Inj.:
1.0µL splitless, double gooseneck inlet liner (cat.# 20784)
Pressure pulse injection, 30psig (0.5min.)
Inj. temp.:
275°C
Carrier gas:
helium, constant flow
Column flow:
1mL/min.
Oven temp.:
35°C (hold 1min.) to 360°C@ 20°C/min. to 330°C@ 6°C/min (hold 1min.)
Det.:
5973MS
Transfer line temp.:
280°C
Scan range:
35-550amu
Ionization:
EI
Mode:
TIC
Figure 1
—Resolve complexmixtures of semivolatileswith an inert, low-bleed column.
