restekadv07 - page 149

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NewAnalytical ReferenceMaterials
ASTMD2887-01, Certified PAHs inDiesel #2, Single Component Explosives,
USEPA 8270 SemivolatilesMegaMix
, Canadian PHC, andMore!
ASTMMethod
D2887-01
CalibrationMixes
pentane (C5)
hexane (C6)
heptane (C7)
octane (C8)
nonane (C9)
decane (C10)
undecane (C11)
dodecane (C12)
tetradecane (C14)
pentadecane (C15)
hexadecane (C16)
heptadecane (C17)
octadecane (C18)
eicosane (C20)
tetracosane (C24)
octacosane (C28)
dotriacontane (C32)
hexatriacontane (C36)
tetracontane (C40)
tetratetracontane (C44)
1%weight each in carbon disulfide, 1g solution/ampul
5%weight each, 1g/ampul
CertifiedPAHs in
Diesel #2
Certified PAHs
Typical Certified Conc. (ppm)
acenaphthene
7
acenaphthylene
1
anthracene
13
fluorene
6
1-methylnaphthalene
110
2-methylnaphthalene
60
naphthalene
30
phenanthrene
13
50,000ppm diesel #2 inmethylene chloride, PAH concentra-
tions listed above, 1mL/ampul
CertifiedAromatics
inGasoline
Certified for:
benzene
ethylbenzene
m
-ethyltoluene
o
-ethyltoluene
p
-ethyltoluene
isopropylbenzene
methyl
tert
-butyl ether
naphthalene
n
-propylbenzene
toluene
1,2,3-trimethylbenzene
1,2,4-trimethylbenzene
1,3,5-trimethylbenzene
m
-xylene
o
-xylene
p
-xylene
5,500ppm gasoline in P&T methanol, certified components
listed, 1mL/ampul
CertifiedBTEX in
UnleadedGas
Composite Standard
Certified for:
benzene
ethylbenzene
isopropyl benzene
methyl
tert
-butyl ether
naphthalene
toluene
m
-xylene
o
-xylene
p
-xylene
5,500ppm gasoline in P&T methanol, certified components
listed, 1mL/ampul
Canadian PHC
• Meets CCME 2001 PetroleumHydrocarbons in Soil
Method–Tier1.
• Primary reference calibration standards for quantifica-
tion of four fractions.
• Meet new requirements for the 2001
revision of ASTM 2887-01.
• Pentane added.
• Equal weight/weight concentrations of all
components—1% or 5%.
• Designed for both calibration and reso-
lution tests—one sample for both test
criteria.
• Confirm diesel #2 TPH and priority PAHs
in a single analysis.
• Certificate of Analysis includes concentra-
tion of TPH and certified concentrations of
individual PAHs.
• Complete data pack available.
with data pack
Each
5-pk.
10-pk.
31673
31673-510
31673-500
31673-520
31773
• Confirm unleaded gasoline TPH, BTEX, and
aromatics in a single analysis.
• Certificate of Analysis includes concentration
of TPH and certified concentrations of BTEX
and individual aromatics.
• Complete data pack available.
with data pack
Each
5-pk.
10-pk.
30485
30485-510
30485-500
30485-520
30585
with data pack
Each
30237
30237-500
5-pk.
30237-510
30237-520
10-pk.
30337
with data pack
Each
5-pk.
10-pk.
31674
31674-510
31674-500
31674-520
31774
with data pack
Each
5-pk.
10-pk.
31675
31675-510
31675-500
31675-520
31775
decane (C10)
hexadecane (C16)
tetratriacontane (C34)
5,000µg/mL each in toluene, 1mL/ampul
CCMEPHCCalibrationMix
pentacontane (C50)
10µg/mL in toluene, 1mL/ampul
C50 in Toluene
with data pack
Each
5-pk.
10-pk.
31684
31684-510
31684-500
31684-520
31784
with data pack
Each
5-pk.
10-pk.
31685
31685-510
31685-500
31685-520
31785
12
s
t
e
p
s
1. Reviewmethod requirements
2. Verify compatibility and stability
3. Test rawmaterials
4. Certify balance andweights
5. Prepare glassware and ampuls
6. Prepare and packagemixture
7. Test to assure quality
8. Validate expiration dates and shelf-life
9. Product packaging
10. Restek documentation
11. ISO 9001 registration
12. Custom referencematerials program
For details on these 12 steps, refer to the annual
Chromatography Products Catalog
(lit. cat.#
59662) or contact Technical Service.
That put
Restek
Reference
Materials
above the rest!
1...,139,140,141,142,143,144,145,146,147,148 150,151,152,153,154,155,156,157,158,159,...297
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