Brominated flame retardantsonanRtx®-1614column.
92
GCCOLUMNS |
APPLICATION-SPECIFICCOLUMNS
Environmental
BrominatedFlameRetardantsAnalysis
Rtx®-1614Columns
(fusedsilica)
(5%phenylmethyl)
• Optimized for PBDE analysis byEPAMethod1614.
• Short columnoption resolves BDE-2093 times faster,with less thermal breakdown.
• Unique deactivation gives higher BDE-209 response, compared toDB-5HT
columns, for greater analytical sensitivity.
• Exceeds EPAMethod1614 resolution criteria forBDE-49 andBDE-71.
1. BDE-10
2. BDE-7
3. BDE-8
4. BDE-11
5. BDE-12
6. BDE-13
7. BDE-15
8. BDE-30
9. BDE-32
10. BDE-17
11. BDE-25
12. BDE-28
13. BDE-33
14. BDE-35
15. BDE-37
16. BDE-75
17. BDE-49
18. BDE-71
19. BDE-47
20. BDE-66
21. BDE-77
22. BDE-100
23. BDE-119
24. BDE-99
25. BDE-116
26. BDE-118
27. BDE-85
28. BDE-155
29. BDE-126
30. BDE-154
31. BDE-153
32. BDE-138
33. BDE-166
34. BDE-183
35. BDE-181
36. BDE-190
37. BDE-208
38. BDE-207
39. BDE-206
40. BDE-209
Column:
Rtx
®
-1614, 15m, 0.25mm ID, 0.10µm (cat.# 10296)
Sample:
100-300ppb PBDE PAR Solution (cat.# EO-5113, Cambridge
Isotope Laboratories Inc.), 500ppb decabromodiphenyl ether
(cat.#BDE-209,Wellington Laboratories)
Inj.:
1µL splitless (hold 1min.), 4mm cyclo double gooseneck
liner (cat.# 20896)
Inj. temp.:
340°C
Carrier gas:
helium, constant flow
Linear velocity: 60cm/sec.@ 120°C
Oven temp.:
120°C (hold 1min.) to 275°C@ 15°C/min. to 300°C@
5°C/min. (hold 5min.)
Detector temp.: µ-ECD@ 345°C
GC_EV01025
Get results3 times
fasterwitha short
columnmethod!
Greatpeak shape
forBDE209!
ID
df
temp. limits
15-Meter
30-Meter
0.25mm 0.10µm -60 to 330/360°C 10296
10295
Tableof Contents for
GCChromatograms
see
page542
Website :
E-mail :
TelNo : 03 9762 2034 . . . inAUSTRALIA
Mar 2011
