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525

REFERENCE STANDARDS |

ENVIRONMENTAL

Pesticides

Pesticides, Chlorinated/Organochlorine/Organohalide,

cont.

04.2, 04.1, 03.2, 3/90, 4/89, and 2/88 SOW (Pesticides), QA Mixes

Pesticide Surrogate Mix

(2 components)

See cat.#s 32000 and 32457 on

page 524

.

1,000 µg/mL in acetone, 1 mL/ampul

cat.# 32017 (ea.)

2,4,5-Trichlorophenol (95-95-4)

Florisil® Cartridge Check Standard

(2,4,5-Trichlorophenol)

In methyl

tert

-butyl ether, 1 mL/ampul

cat.# 32417 (ea.)

4,4'-DDT (50-29-3)

200 µg/mL

Endrin (72-20-8)

100 µg/mL

Organochlorine Pesticide System Evaluation Mix

(2 components)

• Designed for daily assessment of system performance.

• Reveals active sites in the injection port and/or GC column.

• Prepared in MTBE—low expansion volume helps minimize

backflash.

In hexane, 1 mL/ampul

cat.# 32002 (ea.)

α

-BHC (319-84-6)

1 µg/mL

β

-BHC (319-85-7)

1

γ

-BHC (Lindane) (58-89-9)

1

4,4'-DDT (50-29-3)

10

Endrin (72-20-8)

5

Methoxychlor (72-43-5)

25

Pesticide Performance Evaluation Mix

(6 components)

In hexane, 1 mL/ampul

cat.# 32074 (ea.)

α

-BHC (319-84-6)

1 µg/mL

β

-BHC (319-85-7)

1

γ

-BHC (Lindane) (58-89-9)

1

4,4'-DDT (50-29-3)

10

Decachlorobiphenyl (SS) (2051-24-3) 2

Endrin (72-20-8)

5

Methoxychlor (72-43-5)

25

2,4,5,6-Tetrachloro-

m

-xylene (SS)

(877-09-8)

2

Pesticide Performance Evaluation Mix w/Surrogates

(8 components)

Working with solutions containing decachlorobiphenyl

Decachlorobiphenyl has poor solubility in most organic solvents.

The maximum concentration that can be prepared in acetone,

hexane, or isooctane is 200 µg/mL. Temperature will affect the solu-

bility as well. Storing solutions at reduced temperatures will cause

decachlorobiphenyl to precipitate.

Products containing decachlorobiphenyl must be sonicated for a

minimum of 10 minutes prior to opening the ampul. Because each

ultrasonic bath operates at a different energy level, 10 minutes is

a guideline only. Longer sonication time will not affect product

quality.

These precautions apply to working solutions prepared in your

laboratory as well. The amount of compound that precipitates

depends on concentration AND temperature. If you store your

standards at a temperature lower than 4 °C (even dilute solutions),

allow extra sonication time.

tech tip

also available

200+ compound

multiresidue pesticides

standard kits for LC-MS/MS

and GC-MS/MS!

See

pages 568–571 .

200 µg/mL in acetone, 1 mL/ampul

cat.# 32027 (ea.)

200 µg/mL in acetone, 5 mL/ampul

cat.# 32028 (ea.)

2,4,5,6-Tetrachloro-

m

-xylene (877-09-8)

2,4,5,6-Tetrachloro-

m

-xylene

200 µg/mL in acetone, 1 mL/ampul

cat.# 32029 (ea.)

200 µg/mL in acetone, 5 mL/ampul

cat.# 32030 (ea.)

10 µg/mL in isooctane, 1 mL/ampul

cat.# 32289 (ea.)

Decachlorobiphenyl (BZ #209) (2051-24-3)

Decachlorobiphenyl (BZ #209)

200 µg/mL in acetone, 1 mL/ampul

cat.# 32025 (ea.)

Dibutylchlorendate (1770-80-5)

Dibutylchlorendate

CLP Pesticides Mixtures, QA Mixes

In acetone, 1 mL/ampul

cat.# 32018 (ea.)

Aldrin (309-00-2)

25 µg/mL

γ

-BHC (Lindane) (58-89-9)

25

4,4'-DDT (50-29-3)

50

Dieldrin (60-57-1)

50

Endrin (72-20-8)

50

Heptachlor (76-44-8)

25

Pesticide Matrix Spike Mix

(6 components)

For complete listing of PCB reference standards, see pages

530–531.

Low-Concentration Pesticides Mixtures,

QA Mixes

In acetone, 1 mL/ampul

cat.# 32040 (ea.)

γ

-BHC (Lindane) (58-89-9)

10 µg/mL

trans

-Chlordane (5103-74-2)

10

4,4'-DDE (72-55-9)

20

Dieldrin (60-57-1)

20

Endosulfan sulfate (1031-07-8)

20

Endrin (72-20-8)

20

Heptachlor epoxide (isomer B)

(1024-57-3)

10

L/C Pesticide Lab Control Sample

(7 components)