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138
www.restek.comGC COLUMNS |
PACKED/MICROPACKED COLUMNS
Application-Specific Packed/Micropacked Columns
D3606 Application Column Set (2 column set)
• Complete resolution of benzene from ethanol—no compromising coelutions.
• Accurate quantification of benzene and toluene.
• Fully conditioned two column set—ready to use out of the box.
• Listed in the appendix of ASTM Method D3606 as an acceptable alternative to
TCEP columns—get better separation of benzene and ethanol while still following
ASTM method requirements.
Conforms to the specifications established in the current ASTMmethod D3606 for the
quantitation of benzene and toluene in spark ignition fuel containing ethanol.
*Please add column instrument configuration suffix number to cat.# when ordering. See chart on
page 141.
**The column set is designed to accommodate both valve injection and/or syringe injection. Column 1 is configured with
a 2" inlet void to facilitate on-column injection. The inlet is identified on both column 1 and column 2. Note: The inlet of
column 2 is identified for proper orientation for connection to the valve.
Description
cat.#*
price
D3606 Application Column (2 column set)**
Column 1: 6' (1.8 m),
1
/
8
" OD, 2.0 mm ID, nonpolar Rtx-1
Column 2: 16' (4.9 m),
1
/
8
" OD, 2.0 mm ID, proprietary packing material
83606-
Aromatics Analysis
free literature
Resolve Benzene and Toluene
in Spark Ignition Fuels
Containing Ethanol
Download your .
free copy from
lit. cat.# .
PCTS1408-UNV
www.restek.comGasoline Containing Ethanol on D3606 Application Column Set by ASTM D3606-10 (Modified)
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2
4
1
2
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4
6
8
10
Time (min)
GC_PC1224
Column
D3606 application column (2 column set). Column 1: 6' (1.8 m),
1
/
8
" OD, 2.0 mm ID, nonpolar Rtx®-1;
Column 2: 16' (4.9 m),
1
/
8
" OD, 2.0 mm ID, proprietary packing material (cat.# 83606-800)
Sample
Ethanol-containing gasoline with internal standard (IS)
Diluent:
Injection
Sample valve
Sample Loop Vol.: 1.5 µL
Valve Temp.:
150 °C
Oven
Oven Temp.:
135 °C (hold 12 min)
Carrier Gas
He, constant flow
Flow Rate:
20.0 mL/min
Detector
TCD@ 200 °C
Notes
2.38 minute backflush (must be determined for each GC system).
Peaks
1. Ethanol
2. Benzene
3. 2-Butanol (IS)
4. Toluene
Excellent separation of
ethanol and benzene.
Cut time = 2.38 minutes