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58

www.restek.com

GC COLUMNS |

GENERAL-PURPOSE COLUMNS

Stabilwax®

Six columns for the price of five!

Call 800-356-1688, ext. 3, or your Restek

representative for details!

FAMEs in Biodiesel Oils on Stabilwax®

GC_PC00916

Column

Stabilwax®, 30 m, 0.32 mm ID, 0.25 µm (cat.# 10624)

Sample

Tallow source of biodiesel (B100), prepared according

to European Method EN 14103

Injection

Inj. Vol.:

1.0 µL split (split ratio 100:1)

Liner:

Cyclosplitter® (cat.# 20706)

Inj. Temp.:

250 °C

Oven

Oven Temp.:

210 °C (hold 5 min) to 230 °C at 20 °C/min (hold 5 min)

Carrier Gas

H

2

, constant flow

Flow Rate:

3 mL/min

Linear Velocity:

60 cm/sec

Detector

FID@ 250 °C

Peaks

1. Myristic acid

C14:0

2. Palmitic acid

C16:0

3. Palmitoleic acid

C16:1

4. Stearic acid

C18:0

5. Oleic acid

C18:1

6. Linoleic acid

C18:2

7. Linolenic acid

C18:3

8. Arachidic acid

C20:0

9. Gadoleic acid

C20:1

10. Lignoceric acid

C24:0

11. Nervonic acid

C24:1

IS Methyl heptadecanoate

Tallow FAMEs in Biodiesel Oils on Stabilwax®

GC_PC00918

Peaks

1. Myristic acid

C14:0

2. Palmitic acid

C16:0

3. Palmitoleic acid

C16:1

4. Stearic acid

C18:0

5. Oleic acid

C18:1

6. Linoleic acid

C18:2

7. Linolenic acid

C18:3

8. Arachidic acid

C20:0

9. Gadoleic acid

C20:1

10. Behenic acid

C22:0

11. Erucic acid

C22:1

12. Lignoceric acid

C24:0

IS Methyl heptadecanoate

Yellow Grease FAMEs in Biodiesel Oils on Stabilwax®

Visit

www.restek.com

for soy FAMEs and

rapeseed FAMEs analyses.

also

available

Metal MXT® Columns

Rugged, flexible, Siltek®-treated stainless

steel tubing; inertness comparable to

fused silica tubing.

MXT®-WAX columns............

. page 110

Stabilwax® Columns

(fused silica)

(polar phase; Crossbond® polyethylene glycol)

• Rugged enough to withstand repeated water injections.

• Low-bleed PEG column ensures long column lifetimes.

• Temperature range: 40 °C to 260 °C.

• Equivalent to USP G14, G15, G16, G20, and G39 phases.

Restek’s polar-deactivated surface tightly binds the Carbowax® polymer and increases

thermal stability, relative to competitive columns. Because of the increased stability

produced by the bonding process, Stabilwax® columns exhibit long column lifetimes,

even when programming repeatedly up to 260 °C. The bonding mechanism of the

column also produces polar compound retention times that do not shift, as is often

observed on other wax-type columns. In addition, this bonding mechanism produces

a column that can be rejuvenated by solvent washing. Stabilwax® columns are used for

a wide range of compounds and matrices including: FAMEs, flavor compounds, es-

sential oils, solvents, aromatics (including xylene isomers), acrolein/acrylonitrile (EPA

603), and oxygenated compounds. Also used for purity testing of chemicals and ana-

lyzing impurities in water matrices and alcoholic beverages.

Stabilwax® Structure

H

H

C C O

H

H

similar

phases

HP-INNOWax, CP-Wax 52 CB, VF-WAX MS,

ZB-WAXplus

*Maximum temperatures listed are for shorter length columns. Longer columns may have a different maximum temperature.

15-Meter

30-Meter

60-Meter

ID

df

temp. limits

cat.#

price

cat.#

price

cat.#

price

0.25 mm 0.10 µm 40 to 250/260 °C 10605

10608

10611

0.25 µm 40 to 250/260 °C 10620

10623

10626

0.50 µm 40 to 250/260 °C 10635

10638

10641

0.32 mm 0.25 µm 40 to 250/260 °C 10621

10624

10627

0.50 µm 40 to 250/260 °C 10636

10639

10642

1.00 µm 40 to 240/250 °C 10651

10654

10657

0.53 mm 0.25 µm 40 to 250/260 °C 10622

10625

10628

0.50 µm 40 to 250/260 °C 10637

10640

10643

1.00 µm 40 to 240/250 °C 10652

10655

10658

1.50 µm 40 to 230/240 °C 10666

10669

10672

2.00 µm 40 to 220/230 °C 10667

10670

10-Meter

20-Meter

ID

df

temp. limits

cat.#

price

cat.#

price

0.15 mm 0.15 µm 40 to 250/260 °C 43830

43831

0.18 mm 0.18 µm 40 to 250 °C

40602