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488

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REFERENCE STANDARDS |

ENVIRONMENTAL

Gases

Gases

Method 8240

(Volatile Organic Compounds [VOCs])

tech tip

Achieving the Best Results From Gas Standards

In order to achieve the best results from gas standards, proper

handling and storage of gas solutions is of vital importance. Use

the following tips to help ensure trouble-free performance:

• Before opening the sealed ampul, gently invert the ampul .

several times. This will redissolve any gases that may have

migrated into the headspace of the ampul.

• When diluting a gas standard, always add it to a solvent. Adding

the gas standard to an empty vessel prior to adding solvent will

result in the loss of gas compounds.

• Keep the gas standard cold throughout its use. Make sure it is

cold before opening the ampul, work quickly to minimize heat

transfer from hands or room, and only dilute the standard into a

very cold solvent.

• When diluting a gas standard in solvent, make sure the pipette

or needle tip is directly above, or immersed below, the solvent

surface.

• We recommend that any unused portion of gas standard be

disposed of after it has been removed from the sealed ampul.

If it is necessary to store the unused portion, place it into a

tightly capped vial with little to no headspace and store it in the

freezer.

• We recommend that any gas solutions that have been stored

outside of a sealed ampul be disposed of after 7 days.

Spectra (Linde)

104 L Cylinders:

Size: 8 x 24 cm .

Volume/Pressure: .

104 liters of gas .

@ 1,800 psi.

Weight: 1.5 lb/0.7 kg

Scotty (Air Liquide)

110 L Cylinders:

Size: 8.3 x 29.5 cm .

Volume/Pressure: .

110 liters of gas .

@ 1,800 psi.

Weight: 2.2 lb/1 kg.

U.S. DOT Specs: 3AL2216

Cylinder Construction:

aluminum

Cylinder Fitting:

CGA-180 outlet

cylinder design

2,000 µg/mL each in P&T methanol, 1 mL/ampul

cat.# 30020 (ea.)

Bromomethane (methyl bromide) (74-83-9)

Chloroethane (ethyl chloride) (75-00-3)

Chloromethane (methyl chloride) (74-87-3)

Trichlorofluoromethane (CFC-11) (75-69-4)

Vinyl chloride (75-01-4)

624 Calibration Mix #1 (gases)

(5 components)

200 µg/mL each in P&T methanol, 1 mL/ampul

cat.# 30439 (ea.)

2,000 µg/mL each in P&T methanol, 1 mL/ampul

cat.# 30042 (ea.)

Bromomethane (methyl bromide) (74-83-9)

Chloroethane (ethyl chloride) (75-00-3)

Chloromethane (methyl chloride) (74-87-3)

Dichlorodifluoromethane (CFC-12) (75-71-8)

Trichlorofluoromethane (CFC-11) (75-69-4)

Vinyl chloride (75-01-4)

502.2 Calibration Mix #1 (gases)

(6 components)

1 ppm in nitrogen, 104 liters @ 1,800 psi

cat.# 34414 (ea.)

1 ppm in nitrogen, 110 liters @ 1,800 psi

cat.# 26361 (ea.)

1 ppm in nitrogen, 110 liters @ 1,800 psi (Pi-marked cylinder)

cat.# 34414-PI (ea.)

100 ppb in nitrogen, 104 liters @ 1,800 psi

cat.# 34428 (ea.)

100 ppb in nitrogen, 110 liters @ 1,800 psi

cat.# 26362 (ea.)

100 ppb in nitrogen, 110 liters @ 1,800 psi (Pi-marked cylinder)

cat.# 34428-PI (ea.)

No data pack available.

Gas standards are subject to hazardous materials shipping fees by most

freight carriers. All calibration gas standards are nonreturnable due to

DOT hazardous shipping requirements.

Benzene (71-43-2)

Ethylbenzene (100-41-4)

Toluene (108-88-3)

m

-Xylene (108-38-3)

o

-Xylene (95-47-6)

p

-Xylene (106-42-3)

BTEX Gas Mix

(6 components)

1 ppm in nitrogen, 104 liters @ 1,800 psi

cat.# 34418 (ea.)

1 ppm in nitrogen, 110 liters @ 1,800 psi

cat.# 26367 (ea.)

1 ppm in nitrogen, 110 liters @ 1,800 psi (Pi-marked cylinder)

cat.# 34418-PI (ea.)

No data pack available.

Acrylonitrile

Benzene

1,3-Butadiene

Chloroform

1,2-Dichloroethane

Dichloromethane

Tetrachloroethylene

Trichloroethylene

Vinyl chloride

Japan Calibration Mix

(9 components)

For more gas .

calibration .

standards,

see

pages 443–451.

also available

High-Purity VOC Regulators

See

page 453.