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127

GC COLUMNS |

PLOT COLUMNS

Fused Silica Porous Polymer Columns

Rt®-QS-BOND Columns

(fused silica PLOT)

porous divinylbenzene homopolymer

• Intermediate polarity PLOT column incorporating low 4-vinylpyridine.

• Separates ethane, ethylene, and acetylene to baseline.

• Designed for the best possible separation between all C2 isomers.

• Stable to 250 °C.

similar phases

GS-Q

15-Meter

30-Meter

ID

df

temp. limits

cat.#

price

cat.#

price

0.25 mm 8 µm to 250 °C

19767

19768

0.32 mm 10 µm to 250 °C

19739

19740

0.53 mm 20 µm to 250 °C

19737

19738

Solvent Mixture on Rt®-S-BOND

GC_PC01080

Column

Rt®-S-BOND, 30 m, 0.53 mm ID, 20 µm (cat.# 19746)

Sample

Solvent mixture

Injection

Inj. Vol.:

1.0 µL split

Liner:

Taper (4 mm) (cat.# 20798)

Inj. Temp.:

200 °C

Split Vent

Flow Rate:

100 mL/min

Oven

Oven Temp.:

120 °C to 220 °C at 5 °C/min (hold 5.0 min)

Carrier Gas

H

2

, constant pressure (4.2 psi, 29.0 kPa)

Linear Velocity:

40 cm/sec @ 120 °C

Detector

FID@ 220 °C

Peaks

1. Methanol

2. Ethanol

3. Acetonitrile

4. Acetone

5. Dichloromethane

6. 1,1-Dichloroethene

7. Nitromethane

8.

trans

-1,2-Dichloroethylene

9.

cis

-1,2-Dichloroethylene

10. Tetrahydrofuran

11. Chloroform

12. Ethyl acetate

13. 1,2-Dichloroethane

14. 1,1,1-Trichloroethane

15. Benzene

16. 1,2-Dimethoxyethane

17. Trichloroethylene

18. 1,4-Dioxane

19. Pyridine

20. Dimethylformamide

21. Methylcyclohexane

22. Toluene

23. 2-Hexanone

24. Chlorobenzene

25. Ethylbenzene

26.

m

-Xylene

27.

p

-Xylene

28.

o

-Xylene

Rt®-S-BOND Columns

(fused silica PLOT)

porous divinylbenzene homopolymer

• Midpolarity PLOT column, incorporating high 4-vinylpyridine.

• Use for the analysis of nonpolar and polar compounds.

• Stable to 250 °C.

similar

phases

CP-PoraPLOT S

15-Meter

30-Meter

ID

df

temp. limits

cat.#

price

cat.#

price

0.25 mm 8 µm to 250 °C

19769

19770

0.32 mm 10 µm to 250 °C

19747

19748

0.53 mm 20 µm to 250 °C

19745

19746

Refinery Gas Mixture on Rt®-QS-BOND

GC_PC1143

Column

Rt®-QS-BOND, 30 m, 0.53 mm ID, 20 µm (cat.# 19738)

Sample

Refinery gas standard

Injection

Inj. Vol.:

20 µL split

Liner:

2 mm (cat.# 20712)

Inj. Temp.:

200 °C

Split Vent

Flow Rate:

35 mL/min

Oven

Oven Temp.:

40 °C (hold 2 min) to 225 °C at 15 °C/min (hold 5 min)

Carrier Gas

He, constant pressure (11.5 psi, 79.3 kPa)

Linear Velocity:

68 cm/sec @ 40 °C

Detector

TCD@ 225 °C

Make-up Gas

Type:

He

Data Rate:

20 Hz

Sensitivity Mode: He/H

2

Instrument

HP5890 GC

Peaks

1. Air

2. Methane

3. Carbon dioxide

4. Ethylene

5. Acetylene

6. Ethane

7. Propylene

8. Propane

9. Propadiene

10. Isobutane

11. Isobutylene

12. 1-Butene

13. 1,3-Butadiene

14.

n

-Butane

15.

cis

-2-Butene

16.

trans

-2-Butene

17. Isopentane

18. 1-Pentene

19. 2-Methyl-2-

butene

20.

n

-Pentane

21.

cis

-2-Pentene

22.

n

-Hexane