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GC COLUMNS | HIGH-PERFORMANCE Rxi® COLUMNS
Rxi®-5Sil MS
GC_EV00943
Column Rxi®-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm
(cat.# 13623)
Sample 8270 MegaMix® (cat.# 31850)
Benzoic acid (cat.# 31879)
8270 Benzidines mix (cat.# 31852)
Acid surrogate mix (4/89 SOW) (cat.# 31025)
Revised B/N surrogate mix (cat.# 31887)
1,4-Dioxane (cat.# 31853)
SV internal standard mix (cat.# 31206)
Conc.: 10 µg/mL (IS 40 μg/mL)
Injection
Inj. Vol.: 1.0 µL pulsed splitless (hold 0.15 min)
Liner: 4 mm drilled Uniliner® (hole near bottom)
(cat.# 20756)
Inj. Temp.: 250 °C
Pulse Pressure: 25 psi (172.4 kPa)
Pulse Time: 0.2 min
Purge Flow: 60 mL/min
Oven
Oven Temp.: 40 °C (hold 1.0 min) to 280 °C at 25 °C/min
to 320 °C at 5 °C/min (hold 1 min)
Carrier Gas He, constant flow
Flow Rate: 1.2 mL/min
Detector MS
Mode: Scan
Transfer Line Temp.:280 °C
Ionization Mode: EI
Scan Range: 35-550 amu
Peaks
1. 1,4-Dioxane
2. N-Nitrosodimethylamine
3. Pyridine
4. 2-Fluorophenol (SS)
5. Phenol-d6 (SS)
6. Phenol
7. Aniline
8. Bis(2-chloroethyl) ether
9. 2-Chlorophenol
10. 1,3-Dichlorobenzene
11. 1,4-Dichlorobenzene-d4
(IS)
12. 1,4-Dichlorobenzene
13. Benzyl alcohol
14. 1,2-Dichlorobenzene
15. 2-Methylphenol
16. Bis(2-chloroisopropyl)
ether
17. 4-Methylphenol/3-methyl-
phenol
18. N-Nitrosodi-N-propylamine
19. Hexachloroethane
20. Nitrobenzene-d5 (SS)
21. Nitrobenzene
22. Isophorone
23. 2-Nitrophenol
24. 2,4-Dimethylphenol
25. Benzoic acid
26. Bis(2-chloroethoxy)
methane
27. 2,4-Dichlorophenol
28. 1,2,4-Trichlorobenzene
29. Naphthalene-d8 (IS)
30. Naphthalene
31. 4-Chloroaniline
32. Hexachlorobutadiene
33. 4-Chloro-3-methylphenol
34. 2-Methylnaphthalene
35. 1-Methylnaphthalene
36. Hexachlorocyclo
pentadiene
37. 2,4,6-Trichlorophenol
38. 2,4,5-Trichlorophenol
39. 2-Fluorobiphenyl (SS)
40. 2-Chloronaphthalene
41. 2-Nitroaniline
42. 1,4-Dinitrobenzene
43. Dimethyl phthalate
44. 1,3-Dinitrobenzene
45. 2,6-Dinitrotoluene
46. 1,2-Dinitrobenzene
47. Acenaphthylene
48. 3-Nitroaniline
49. Acenaphthene-d10 (IS)
50. Acenaphthene
51. 2,4-Dinitrophenol
52. 4-Nitrophenol
53. 2,4-Dinitrotoluene
54. Dibenzofuran
55. 2,3,5,6-Tetrachlorophenol
56. 2,3,4,6-Tetrachlorophenol
57. Diethyl phthalate
58. 4-Chlorophenyl phenyl
ether
59. Fluorene
60. 4-Nitroanaline
61. 4,6-Dinitro-2-
methylphenol
62. n -Nitroso-diphenylamine
(diphenylamine)
63. 1,2-Diphenylhydrazine
(as azobenzene)
64. 2,4,6-Tribromophenol (SS)
65. 4-Bromophenyl phenyl
ether
66. Hexachlorobenzene
67. Pentachlorophenol
68. Phenanthrene-d10 (IS)
69. Phenanthrene
70. Anthracene
71. Carbazole
72. di-n -Butyl phthalate
73. Fluoranthene
74. Benzidine
75. Pyrene-d10 (SS)
76. Pyrene
77. p -Terphenyl-d14 (SS)
78. 3,3'-Dimethylbenzidine
79. Butyl benzyl phthalate
80. Bis(2-ethylhexyl) adipate
81. 3,3'-Dichlorobenzidine
82. Benzo[a]anthracene
83. Bis(2-ethylhexyl)phthalate
84. Chrysene-d12 (IS)
85. Chrysene
86. Di- n -octyl phthalate
87. Benzo[b]fluoranthene
88. Benzo[k]fluoranthene
89. Benzo[a]pyrene
90. Perylene-d12 (IS)
91. Indeno[1,2,3-cd]pyrene
92. Dibenzo[a,h]anthracene
93. Benzo[ghi]perylene
c = contaminant (toluene)
Semivolatiles by EPA Method 8270 on Rxi®-5Sil MS (30 m, 0.25 mm ID, 0.25 µm) w/Drilled Uniliner® Inlet Liner